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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Cannio, M.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2022Insight into t->m transition of MW treated 3Y-PSZ ceramics by grazing incidence X-ray diffractioncitations
- 2021Electrophoretic deposition: An effective technique to obtain functionalized nanocoatingscitations
- 2018Microstructure and engineering properties of Fe2O3(FeO)-Al2O3-SiO2 based geopolymer compositescitations
- 2016Investigation of the bonding strength and bonding mechanisms of SOFCs interconnector-electrode interfacescitations
- 2015Ultrafast microwave hydrothermal synthesis and characterization of Bi1-xLaxFeO3 micronized particlescitations
- 2014Metakaolin-based inorganic polymer composite: Effects of fine aggregate composition and structure on porosity evolution, microstructure and mechanical propertiescitations
- 2013Effect of low-temperature high-pressure sintering on BiFeO3 density, electrical magnetic and structural propertiescitations
- 2008Service life prediction for refractory materialscitations
- 2006Physical-chemical characterization of a galvanic sludge and its inertization by vitrification using container glasscitations
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article
Ultrafast microwave hydrothermal synthesis and characterization of Bi1-xLaxFeO3 micronized particles
Abstract
In this work a microwave assisted hydrothermal method is applied to successfully synthesize lanthanum doped bismuth ferrites (BLFO, Bi1-xLaxFeO3 where x = 0, 0.15, 0.30 and 0.45). The growth mechanism of the Bi1-xLaxFeO3 crystallites is discussed in detail. The existence of the single-phase perovskite structure for all the doped samples is confirmed by the X-ray powder diffraction patterns. A peak shift, observed at lower angle with increasing La doping concentration, indicates that the BiFeO3 lattice is doped. The results of TG/DTA show a shift in the transition temperature from 805 degrees C to 815 degrees C as function of the La-doping for all the doped powders. At higher levels of La doping, i.e. x = 0.30 and 0.45, significant weight losses occur above 860 degrees C suggesting a change in the physical and chemical properties. Finally, magnetic measurements are carried out at room temperature for pure BiFeO3 and Bi0,83La0.15FeO3. The results indicate that the materials are both weakly ferromagnetic, with no significant hysteresis in the curves. (C) 2015 Elsevier B.V. All rights reserved.