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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Martinez-Tejada, Hader Vladimir
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2018Effect of the tryptone concentration on the calcium carbonate biomineralization mediated by Bacillus cereuscitations
- 2018Synthesis and morphological characterization of Li-Ti/PVP fibers as precursors for Li4Ti5O12 towards its future use as anode materials in Li-ion fiber batteries by means of Electrospinningcitations
- 2018Structural health monitoring using carbon nanotube/epoxy composites and strain-field pattern recognition
- 2018Electrospinning synthesis of Li-Fe-P/PAN based micro-nanofibers as precursors for LiFePO4 cathode material in Li-ion fiber battery applicationscitations
- 2017Solid-state fabrication of Al/CNTs nanocompositescitations
- 2017Computational simulation of a diffusion process of carbon nanotubes in aluminium to improve the mechanical properties of a composite material
- 2013Synthesis and investigation of PMMA films with homogeneously dispersed multiwalled carbon nanotubescitations
- 2012Characterization and electrocatalytic properties of sonochemical synthesized PdAg nanoparticlescitations
- 2009Consolidation of carbon nanofiber/copper composites by hot-pressing and spark plasma sinteringcitations
- 2008One-step SSM process by MSC & HPDC for metallic components
- 2006Constitutive model of the alloy 2117-T4 at low strain rates and temperaturescitations
- 2005PRODUCCIÓN Y CARACTERIZACIÓN DE PARTÍCULAS Y FIBRAS CORTAS DE β-SiC OBTENIDAS A PARTIR DE CÁSCARA DE ARROZ. (Spanish)
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article
Synthesis and investigation of PMMA films with homogeneously dispersed multiwalled carbon nanotubes
Abstract
<p>Multiwalled carbon nanotubes (MWNT) modified by 2.2′-azoiso- butyronitrile (AIBN) were incorporated into methyl methacrylate (MMA) by sonochemistry method, resulting in homogenous dispersion of MWNT, which makes possible to obtain flexible conductive polymer-matrix nanocomposites films of PMMA, with MWNT concentrations ranging from 0 to 0.5 wt%. Modified MWNT (AIBN-MWNT) were studied by Fourier transform infrared (FT-IR), Raman spectroscopy, X-ray Photoelectron Spectroscopy (XPS) and through visual observations in order to compare the dispersion in 2-propanone and toluene with that of pristine MWNT. Synthesized PMMA-AIBN-MWNT films were studied by FT-IR and Raman spectroscopy. Using FT-IR for the AIBN-MWNT it was not possible to identify any group or groups attached to the nanotubes. Raman spectroscopy shows a small modification in the Lorentzian peaks ratio I<sub>D/G</sub> of AIBN-MWNT, meanwhile XPS showed that atomic compositions does not change for AIBN-MWNT compared to the pristine nanotubes. Also by impedance it was analyzed the conductivity of PMMA-MWNT films and the results showed a threshold percolation at 0.5 wt%. FT-IR and Raman analyses for PMMA-AIBN-MWNT composite indicate a covalent bonding between PMMA and MWNT due to the opening of π-bonds of the nanotubes, which is related with a possible proposed reaction scheme.</p>