| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Donoghue, Jack
University of Manchester
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (29/29 displayed)
- 2024In-situ Heating-Stage EBSD Validation of Algorithms for Prior Austenite Grain Reconstruction in Steelcitations
- 2024Exploration of fs-laser ablation parameter space for 2D/3D imaging of soft and hard materials by tri-beam microscopycitations
- 2024Grain-scale in-situ study of discontinuous precipitation in Mg-Alcitations
- 2024Understanding Ag liquid migration in SiC through ex-situ and in-situ Ag-Pd/SiC interaction studiescitations
- 2024Identification, classification and characterisation of hydrides in Zr alloyscitations
- 2024Identification, classification and characterisation of hydrides in Zr alloys
- 2024Biomimetic dual sensing polymer nanocomposite for biomedical applicationscitations
- 2023Development of a high strength liquid assisted healable modified AlMg alloy produced by additive manufacturing
- 2023Development of a high strength liquid assisted healable modified AlMg alloy produced by additive manufacturing
- 2023Characterization of Hydride Precipitation and Reorientation in Zircaloy-4 at Different Metallurgical States
- 2023Mitigation effects of over-aging (T73) induced intergranular corrosion on stress corrosion cracking of AA7075 aluminum alloy and behaviors of η phase grain boundary precipitates during the intergranular corrosion formationcitations
- 2023Development of a new healable aluminium alloy produced by Laser Powder Bed Fusion (LPBF) and improvement of its strength through strengthening element addition
- 2022Large-scale serial sectioning of environmentally assisted cracks in 7xxx Al alloys using femtosecond Laser-PFIBcitations
- 2022Large-scale serial sectioning of environmentally assisted cracks in 7xxx Al alloys using femtosecond Laser-PFIBcitations
- 2022Multi-dimensional study of the effect of early slip activity on fatigue crack initiation in a near-α titanium alloycitations
- 2022Optimising large-area crystal orientation mapping of nanoscale β phase in α + β titanium alloys using EBSDcitations
- 2022CHARACTERISATION OF HYDRIDE PRECIPITATION AND REORIENTATION IN ZIRCALOY-4 AT DIFFERENT METALLURGICAL STATES
- 2021In-Situ Observation of Single Variant α Colony Formation in Ti-6Al-4Vcitations
- 2021Multiscale analysis of grain boundary microstructure in high strength 7xxx Al alloyscitations
- 2020On the Observation of Annealing Twins during Simulating β-Grain Refinement in Ti-6Al-4V High Deposition Rate AM with In-Process Deformationcitations
- 2020Measurement of local plastic strain during uniaxial reversed loading of nickel alloy 625
- 2020Tracking polycrystal evolution non-destructively in 3D by laboratory X-ray diffraction contrast tomographycitations
- 2020On the observation of annealing twins during simulating β-grain refinement in Ti–6Al–4V high deposition rate AM with in-process deformationcitations
- 2019On the application of Xe+ plasma FIB for micro-fabrication of small-scale tensile specimenscitations
- 2019On the application of Xe+ plasma FIB for micro-fabrication of small-scale tensile specimenscitations
- 2019Data for Indirect to direct gap crossover in two-dimensional InSe revealed by angle resolved photoemission spectroscopy
- 2019Indirect to direct gap crossover in two-dimensional InSe revealed by angle-resolved photoemission spectroscopycitations
- 2016The Effectiveness of Combining Rolling Deformation with Wire-Arc Additive Manufacture on β -Grain Refinement and Texture Modification in Ti-6Al-4Vcitations
- 2015Integration of Deformation Processing with Additive Manufacture of Ti-6Al-4V Components for Improved β Grain Structure and Texture
Places of action
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article
Optimising large-area crystal orientation mapping of nanoscale β phase in α + β titanium alloys using EBSD
Abstract
α + β titanium alloys, such as the commercially important alloy Ti-6Al-4 V (Ti64), develop complex textures during thermomechanical processing due to the allotropic phase transformation between the β and α phases. These phases are crystallographically related through the Burgers orientation relationship (BOR) and are often characterised by electron backscatter diffraction (EBSD) in the scanning electron microscope (SEM). However, the BOR can be destroyed for the primary α in wrought Ti64, and techniques that utilise the BOR to reconstruct the β phase from the room temperature α-phase data cannot be used. Instead, the β texture must be measured from the residual, nanoscale β ligaments in the room temperature microstructure, which are challenging to index because of orientation and phase overlap in the EBSD Kikuchi patterns. In this work, the SEM-EBSD acquisition and processing parameters were systematically varied to determine how best to index the residual β in Ti64, and an experimental methodology was thus developed to measure the β-phase texture efficiently and reliably after thermomechanical processing. The best compromise for maximising indexing of the residual β was achieved with a low current (~1 nA in this case), and additional indexing was achieved by increasing the sample stage tilt (to 75° in this case) and by limited the scanning frame size. It was shown that the β-phase texture could be reliably measured with the optimised beam and tilt settings using a relatively coarse step size (3 μm), but this approach does not yield any morphological or spatially relevant microstructure data. Thus, it was proposed that numerous multi-scale scans be performed with different settings to characterise the residual β phase in T64, each optimised to acquire either bulk texture analysis or microstructure spatial and morphological detail.