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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Presoly, Peter
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (25/25 displayed)
- 2024Experimental investigation and computational thermodynamics of the quaternary system Fe-C-Mn-S
- 2024On the Role of Tramp Elements for Surface Defect Formation in Continuous Casting of Steelcitations
- 2024Influence of Silicon and Tramp Elements on the High-temperature Oxidation of Steel in Direct Casting and Rolling Processes
- 2024Critical Examination of the Representativeness of Austenite Grain Growth Studies Performed In Situ Using HT-LSCM and Application to Determine Growth-inhibiting Mechanismscitations
- 2023The influence of intergranular oxidation on surface crack formation in continuous casting of steelcitations
- 2023Classification of peritectic steels by experimental methods, computational thermodynamics and plant data: An Overview
- 2023Thermodynamic modeling of the Fe-Sn system including an experimental re-assessment of the liquid miscibility gapcitations
- 2023Decomposition of γ-Fe in 0.4C-1.8Si-2.8Mn-0.5Al steel during a continuous cooling process: A comparative study using in-situ HT-LSCM, DSC and dilatometrycitations
- 2023High-temperature oxidation of steel recycled from scrap: The role of tramp elements and their influence on oxidation behavior
- 2022High temperature thermodynamics of the Fe-C-Mn system; new experimental data for the Fe-C-10 and 20 wt.-% Mn system
- 2022Primary Carbide Formation in Tool Steelscitations
- 2022Evaluation of different alloying concepts to trace non-metallic inclusions by adding rare earths on a laboratory scalecitations
- 2022Selected metallurgical models for computationally efficient prediction of quality-related issues in continuous slab casting of steel
- 2022Experimental thermodynamics for improving CALPHAD optimizations at the Chair of Ferrous Metallurgy
- 2021Characterization of the gamma-loop in the Fe-P system by coupling DSC and HT-LSCM with complementary in-situ experimental techniquescitations
- 2020Study on the Possible Error Due to Matrix Interaction in Automated SEM/EDS Analysis of Nonmetallic Inclusions in Steel by Thermodynamics, Kinetics and Electrolytic Extractioncitations
- 2020Experimental Study of High Temperature Phase Equilibria in the Iron-Rich Part of the Fe-P and Fe-C-P Systemscitations
- 2020Investigation of Fe–C–Cr and Fe–C–Cr–Ni-based systems with the use of DTA and HT-LSCM methodscitations
- 2019High precious phase diagrams – a roadmap for a successful casting processing
- 2019Evaluation of AHSS concepts with a focus on the product properties and appropriate casting characteristics of Arvedi ESP thin slab casterscitations
- 2017The potential for grain refinement of a super austenitic stainless steel with a cerium grain refiner
- 2017Modeling Inclusion Formation during Solidification of Steelcitations
- 2017Influence of Silicon and Manganese on the Peritectic Range for Steel Alloys
- 2017Further development and validation of IDS by means of selected experiments
- 2016On the modelling of microsegregation in steels involving thermodynamic databases
Places of action
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article
Characterization of the gamma-loop in the Fe-P system by coupling DSC and HT-LSCM with complementary in-situ experimental techniques
Abstract
<p>Solid-state phase transformations in the γ-loop of the binary Fe-P system were studied using differential scanning calorimetry (DSC) and high-temperature laser scanning confocal microscopy (HT-LSCM). In total, eight alloys with varying P content from 0.026 to 0.48 mass pct. P were investigated in the temperature range of 800 °C to 1450 °C. The first part of the present work deals with the critical evaluation of the approach to couple DSC experiments and HT-LSCM observations in order to characterize bcc/fcc phase equilibria in Fe-based γ-loops. The phase transformation temperatures of a selected alloy with 0.394%P were analyzed by DSC and HT-LSCM and compared with results of the well-established techniques of dilatometry and high-temperature X-ray diffraction (HT-XRD). Then, the overall phase boundaries of the γ-loop were reconstructed by HT-LSCM and DSC data and the phase diagram was compared with thermodynamic assessments from literature. Finally, the quantitative phase fractions of fcc and bcc at 0.394%P were analyzed by Rietveld refinement at temperatures of 1050 °C, 1100 °C and 1150 °C using in-situ HT-XRD. Although the phase boundaries of the γ-loop and phase transformation temperatures have been reproduced accurately by recently published thermodynamic optimizations, larger deviations between HT-XRD measurements and the calculations were identified for the phase fraction prediction. The present work clearly demonstrates that coupling DSC and HT-LSCM is a powerful tool to characterize γ-loops in steel for future research work.</p>