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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Nießen, Frank
Technical University of Denmark
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (23/23 displayed)
- 2024Efficient ab initio stacking fault energy mapping for dilute interstitial alloyscitations
- 2024Residual Stress Measurement across the Scales
- 2023Reconciling experimental and theoretical stacking fault energies in face-centered cubic materials with the experimental twinning stresscitations
- 2023Aging 17-4 PH martensitic stainless steel prior to hardeningcitations
- 2023Ab initio study of the effect of interstitial alloying on the intrinsic stacking fault energy of paramagnetic γ-Fe and austenitic stainless steelcitations
- 2022High resolution crystal orientation mapping of ultrathin films in SEM and TEMcitations
- 2021Parent grain reconstruction from partially or fully transformed microstructures in MTEX
- 2021Experimental validation of negative stacking fault energies in metastable face-centered cubic materialscitations
- 2021Multiscale in-situ studies of strain-induced martensite formation in inter-critically annealed extra-low-carbon martensitic stainless steelcitations
- 2020Strain, stress and stress relaxation in oxidized ZrCuAl-based bulk metallic glasscitations
- 2020Strain, stress and stress relaxation in oxidized ZrCuAl-based bulk metallic glasscitations
- 2020Evolution of substructure in low-interstitial martensitic stainless steel during temperingcitations
- 2018In-situ analysis of redistribution of carbon and nitrogen during tempering of low interstitial martensitic stainless steelcitations
- 2018Martensite Formation from Reverted Austenite at Sub-zero Celsius Temperaturecitations
- 2018In Situ Investigation of the Evolution of Lattice Strain and Stresses in Austenite and Martensite During Quenching and Tempering of Steelcitations
- 2018Formation and stabilization of reverted austenite in supermartensitic stainless steelcitations
- 2018Phase Transformations in Supermartensitic Stainless Steels
- 2017Kinetics analysis of two-stage austenitization in supermartensitic stainless steelcitations
- 2017Complementary Methods for the Characterization of Corrosion Products on a Plant-Exposed Superheater Tubecitations
- 2017Complementary Methods for the Characterization of Corrosion Products on a Plant-Exposed Superheater Tubecitations
- 2017Formation and stabilization of reversed austenite in supermartensitic stainless steel
- 2017Kinetics modeling of delta-ferrite formation and retainment during casting of supermartensitic stainless steelcitations
- 2016In Situ Techniques for the Investigation of the Kinetics of Austenitization of Supermartensitic Stainless Steelcitations
Places of action
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article
Evolution of substructure in low-interstitial martensitic stainless steel during tempering
Abstract
The evolution of the substructure and the distribution of interstitial elements in lath martensite during tempering in soft martensitic stainless steel X4CrNiMo16-5-1 was studied with line profile analysis of diffractograms from energy dispersive synchrotron X-ray diffraction, local chemical analysis with atom probe tomography and orientation mapping with electron backscatter and transmission Kikuchi diffraction. Martensite formation occurred below 135 °C without auto-tempering and led to a dislocation density in martensite of 3.8 ∙ 10 15 m −2 , as determined from X-ray line profile analysis. On tempering, carbon and nitrogen segregated to low-angle and high-angle grain boundaries. Recovery commenced above 550 °C and led to a reduction in dislocation density to a steady value of 4 ∙ 10 14 m −2 from 600 to 750 °C. Further tempering led to a second increase in dislocation density at room temperature, owing to the transformation of reverted austenite, formed above 650 °C, into martensite on cooling. It was observed that the recovery of martensite competes with the formation of reverted austenite. The interpretation of the coherently diffracting domain size obtained from X-ray line profile analysis was critically discussed in the context of the internal structure in martensite.