| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Ravnsbæk, Dorthe Bomholdt
Aarhus University
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (14/14 displayed)
- 2023All-solid-state sodium-ion batteries operating at room temperature based on NASICON-type NaTi2(PO4)3 cathode and ceramic NASICON solid electrolytecitations
- 2022An Easy‐to‐Use Custom‐Built Cell for Neutron Powder Diffraction Studies of Rechargeable Batteriescitations
- 2021Synthesis and Thermal Degradation of MAl4(OH)12SO4·3H2O with M = Co2+, Ni2+, Cu2+, and Zn2+citations
- 2021Understanding disorder in oxide-based electrode materials for rechargeable batteriescitations
- 2021Synthesis and Thermal Degradation of MAl 4 (OH) 12 SO 4 ·3H 2 O with M = Co 2+ , Ni 2+ , Cu 2+ , and Zn 2+citations
- 2020The Effect of oxygen defects on the structural evolution of LiVPO4F1−yoy cathode materialscitations
- 2020On the synthesis and structure of the copper-molybdenum oxide bronzes
- 2017Synthesis, structure and properties of bimetallic sodium rare-earth (RE) borohydrides, NaRE(BH4)4, RE = Ce, Pr, Er or Gdcitations
- 2017Nanoconfined NaAlH4 Conversion Electrodes for Li Batteriescitations
- 2016Synthesis, structure and properties of new bimetallic sodium and potassium lanthanum borohydridescitations
- 2015Manganese borohydride; synthesis and characterizationcitations
- 2014A novel intermediate in the LiAlH4–LiNH2 hydrogen storage systemcitations
- 2014Hydrogen reversibility of LiBH₄-MgH₂-Al compositescitations
- 2011Novel metal boroydrides: Studies of synthesis, crystal chemistry and thermal decomposition
Places of action
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article
On the synthesis and structure of the copper-molybdenum oxide bronzes
Abstract
<p>Cu<sub>2</sub>Mo<sub>10</sub>O<sub>30</sub> was prepared as a monophasic material comprising dark blue platy crystals by reacting Cu with MoO<sub>3</sub> under argon at 550 °C. Single-crystal X-ray diffractometry showed that Cu<sub>2</sub>Mo<sub>10</sub>O<sub>30</sub> is a stoichiometric compound that crystallizes with a monoclinic (C2/c) cell: a = 16.6359(6); b = 9.3112(3); c = 27.1597(9) Å; β = 102.621(3)° (Z = 8). Electron paramagnetic resonance spectroscopy revealed that Cu<sub>2</sub>Mo<sub>10</sub>O<sub>30</sub> displays mixed-valency; (Cu<sup>I</sup> <sub>2−x</sub>Cu<sup>II</sup> <sub>x</sub>)(Mo<sup>V</sup> <sub>2+x</sub>Mo<sup>VI</sup> <sub>8−x</sub>)O<sub>30</sub> (0 ≪ x ≤ 2). Differential scanning calorimetry and in situ high-temperature powder X-ray diffractometry showed that Cu<sub>2</sub>Mo<sub>10</sub>O<sub>30</sub> decomposes ≳550 °C under an inert atmosphere. Dark blue acicular crystals of CuMo<sub>9</sub>O<sub>26</sub> were discovered as a side-product in materials prepared inside evacuated glass ampoules at 500 °C. Single-crystal X-ray diffractometry showed these to crystallize with an orthorhombic (Pmmn) cell: a = 3.74190(10); b = 26.4941(4); c = 9.15300(10) Å; (Z = 2). Rietveld refinement of the powder X-ray diffraction data for these materials revealed Cu<sub>2</sub>Mo<sub>10</sub>O<sub>30</sub> with minor CuMo<sub>9</sub>O<sub>26</sub> and ‘Cu<sub>0.1</sub>MoO<sub>3</sub>’.</p>