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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Torvisco, Ana
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2024Synthesis and Characterization of Alkali Metal Hypersilyl Borates
- 2023Dinuclear doubly bridged phenoxido copper(II) complexes as efficient anticancer agentscitations
- 2023Synthesis and Characterization of 3-Aminopropyl-phenyl Germanescitations
- 2023Structure and magnetic characterization of some bicompartmental [N6O2] divalent metal(ii) complexes using bis(phenolato) ligands bearing two pendant bis(pyridyl) amine arms
- 2023Magnetostructural Properties of Some Doubly-Bridged Phenoxido Copper(II) Complexescitations
- 2023Copper(II) and zinc(II) complexes bridged by benzenoid aromatic oxocarbon and dicarboxylate dianionscitations
- 2021Syntheses, structural characterization, and thermal behaviour of metal complexes with 3-aminopyridine as co-ligandscitations
- 2020Synthesis and characterization of zinc di(O-2,2-dimethylpentan-3-yl dithiocarbonates) bearing pyridine or tetramethylethylenediamine coligands and investigation of their thermal conversion mechanisms towards nanocrystalline zinc sulfidecitations
- 2020Polynuclear and coordination polymers of copper(II) complexes assembled by flexible polyamines and bridging rigid N-heterocyclic multicarboxylatescitations
- 2019Structure, DFT Calculations, and Magnetic Characterization of Coordination Polymers of Bridged Dicyanamido-Metal(II) Complexescitations
- 2019Synthesis and characterization of 1D coordination polymers of metal(II)-dicyanamido complexescitations
- 2014Stable Silenolates and Brook-Type Silenes with Exocyclic Structurescitations
- 2014Photoinduced Brook-type Rearrangement of Acylcyclopolysilanescitations
- 2013Bismuth sulphide–polymer nanocomposites from a highly soluble bismuth xanthate precursorcitations
- 2013Synthesis and Properties of Bridgehead-Functionalized Permethylbicyclo[2.2.2]octasilanescitations
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article
Synthesis and Characterization of 3-Aminopropyl-phenyl Germanes
Abstract
<p>Novel synthetic pathways for different 3-aminopropyl germanes are shown in this work. For this purpose, in Synthetic Route A, a corresponding germanium compound was metalated and, via salt metathesis, the corresponding protected 3-aminopropyl germane was formed. After the deprotection, the corresponding amino hydrochlorides were isolated. After a neutralization reaction, the 3-aminopropyl germanes were formed. With 3-aminopropyl-diphenyl-germanium hydride, (H<sub>2</sub>N(CH<sub>2</sub>)<sub>3</sub>)Ph<sub>2</sub>GeH, a new bifunctional building block was isolated. To form the corresponding 3-aminopropyl‑chloro germanes ((CyHN(CH<sub>2</sub>)<sub>3</sub>)Ph<sub>2</sub>GeCl and (H<sub>2</sub>N(CH<sub>2</sub>)<sub>3</sub>)Ph<sub>2</sub>GeCl), diphenyl‑chloro germane was used in a hydrogermylation to form the corresponding amines (Synthetic Route B). All compounds were characterized by state-of-the-art techniques, including single crystal X-ray diffraction for selected compounds.</p>