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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Lima, Maria Margarida Rolim Augusto
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (17/17 displayed)
- 2018Thermal characteristics and crystallization behavior of zinc borosilicate glasses containing Nb2O5citations
- 2016Formation and crystallization of zinc borosilicate glassescitations
- 2015Crystallization of lithium disilicate-based multicomponent glasses - effect of silica/lithia ratiocitations
- 2014Crystallization kinetics of a barium-zinc borosilicate glass by a non-isothermal methodcitations
- 2014Phase transformation and microstructural evolution after heat treatment of a terbium-doped lithium–aluminum phosphate glasscitations
- 2014Synthesis of Niobium Doped Zinc Borosilicate Glass-ceramics
- 2014Crystallization and microstructure of Eu3+-doped lithium aluminophosphate glasscitations
- 2014Glass transition and crystallization kinetics of a barium borosilicate glass by a non-isothermal methodcitations
- 2014A novel dental restorative glass-ceramic based on fluorcanasite
- 2013Rare-earth doped phosphate glasses
- 2013Crystallization kinetics terbium-doped aluminophosphate glass studied by DSC, XRD and SEM
- 2013Effect of Phosphogypsum on the Clinkerization Temperature of Portland Cement Clinkercitations
- 2012Sintering,Crystallization and Dielectric Behavior of Barium Zinc Borosilicate Glasses - Effect of Barium Oxide substitution for Zinc Oxidecitations
- 2012Structural, electrical and thermal properties of borosilicate glass-alumina compositescitations
- 2008Mechanical characteristics of clay structural ceramics containing coal fly ashcitations
- 2004Recycling of coal fly ash by ceramic processing
- 2000Pressureless sintering of alumina-glass compositescitations
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article
Formation and crystallization of zinc borosilicate glasses
Abstract
<p>Different glasses based on the ZnO-B<sub>2</sub>O<sub>3</sub>-SiO<sub>2</sub> system, with a ZnO content ≥ 60 mol% and a fixed SiO<sub>2</sub> content (20 mol%), were synthesised using a melt-quenching method. Glass samples with zinc oxide concentrations as high as 65 mol% were prepared successfully without deteriorating the glass-forming ability. The glass samples were submitted to controlled heat-treatments, and the effect of the ZnO/B<sub>2</sub>O<sub>3</sub> molar ratio on the formation of crystalline phases within the glass matrix was investigated by means of differential thermal analysis (DTA), X-ray diffraction (XRD) and scanning electron microscopy (SEM). DTA results indicated that the glass transition and the onset crystallization temperatures of the studied glasses tended to increase with the increment on the ZnO/B<sub>2</sub>O<sub>3</sub> ratio. XRD data showed that the zinc binary crystalline phases, willemite (Zn<sub>2</sub>SiO<sub>4</sub>), a zinc orthosilicate, and zinc borate (Zn<sub>3</sub>B<sub>2</sub>O<sub>6</sub>) could be present in the crystallized glasses, depending on the heat-treatment conditions. The formation of willemite was promoted by an increasing ZnO/B<sub>2</sub>O<sub>3</sub> ratio. Microstructural observations performed by SEM indicated that under controlled experimental parameters (glass composition, heat-treatment temperature and time) the precipitation of nanocrystals within the glass matrix can be achieved, resulting in transparent and translucent willemite glass-ceramics.</p>