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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Sheridan, Richard
University of Birmingham
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (16/16 displayed)
- 2024Strip Casting of Sm2TM17-Type Alloys for Production of the Metastable SmTM7 Phase
- 2024Development of anisotropic Nd-Fe-B powder from isotropic gas atomized powdercitations
- 2023Strip Casting of Sm2TM17-type Alloys for Production of the Metastable SmTM7 Phase
- 2023On the origin of cracking in laser powder bed fusion processed LaCe(Fe,Mn,Si)13, and the impact of post-processingcitations
- 2023The effect of thermal post-processing treatment on laser powder bed fusion processed NiMnSn-based alloy for magnetic refrigerationcitations
- 2022The effect of grain size on the internal oxidation of Sm2Co17-type permanent magnetscitations
- 2021Microstructure-magnetic shielding development in additively manufactured Ni-Fe-Mo soft magnet alloy in the as fabricated and post-processed conditionscitations
- 2020Limitations in grain boundary processing of the recycled HDDR Nd-Fe-B systemcitations
- 2020Magnetic shielding promotion via the control of magnetic anisotropy and thermal Post processing in laser powder bed fusion processed NiFeMo-based soft magnetcitations
- 2020The extraction of NdFeB magnets from automotive scrap rotors using hydrogencitations
- 2019Magnetic properties of REE fluorcarbonate minerals and their implications for minerals processingcitations
- 2019Coercivity increase of the recycled HDDR Nd-Fe-B powders doped with DyF3 and processed via Spark Plasma Sintering & the effect of thermal treatmentscitations
- 2016REE Recovery from End-of-Life NdFeB Permanent Magnet Scrap: A Critical Reviewcitations
- 2016The development of microstructure during hydrogenation–disproportionation–desorption–recombination treatment of sintered neodymium-iron-boron-type magnetscitations
- 2016Novel "Flash Spark Plasma Sintering" method for the rapid fabrication of nanostructured and anisotropic rare-earth lean permanent magnetic materials
- 2014The Effect of Ni Impurities on HDDR Processing of Scrap Sintered NdFeB Magnets
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article
The development of microstructure during hydrogenation–disproportionation–desorption–recombination treatment of sintered neodymium-iron-boron-type magnets
Abstract
The hydrogen absorption and desorption characteristics of the hydrogenation disproportionation desorption and recombination (HDDR) process on scrap sintered neodymium-iron-boron (NdFeB) type magnets have been investigated. At each stage of the process, the microstructural changes have been studied using high resolution scanning electron microscopy. It was found that the disproportionation reaction initiates at grain boundaries and triple points and then propagates towards the centre of the matrix grains. This process was accelerated at particle surfaces and at free surfaces produced by any cracks in the powder particles. However, the recombination reaction appeared to initiate randomly throughout the particles with no apparent preference for particle surfaces or internal cracks. During the hydrogenation of the grain boundaries and triple junctions, the disproportionation reaction was, however, affected by the much higher oxygen content of the sintered NdFeB compared with that of the as-cast NdFeB alloys. Throughout the entire HDDR reaction the oxidised triple junctions (from the sintered structure) remained unreacted and hence, remained in their original form in the fine recombined microstructure. This resulted in a very significant reduction in the proportion of cavitation in the final microstructure and this could lend to improved consolidation in the recycled magnets.