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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Schwaiger, Ruth
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (25/25 displayed)
- 2024Enabling High-Performance Hybrid Solid-State Batteries by Improving the Microstructure of Free-Standing LATP/LFP Composite Cathodes
- 2024Controlling shear band instability by nanoscale heterogeneities in metallic nanoglasses
- 2024Microstructure Characterization and Mechanical Properties of Polymer‐Derived (HfₓTa₁₋ₓ)C/SiC Ceramic Prepared upon Field‐Assisted Sintering Technique/Spark Plasma Sintering
- 2024Enabling High-Performance Hybrid Solid-State Batteries by Improving the Microstructure of Free-Standing LATP/LFP Composite Cathodes.citations
- 2024Comparative Study of High-Cycle Fatigue and Failure Mechanisms in Ultrahigh-Strength CrNiMoWMnV Low-Alloy Steels
- 2024Microstructure Characterization and Mechanical Properties of Polymer‐Derived (Hf<sub><i>x</i></sub>Ta<sub>1−<i>x</i></sub>)C/SiC Ceramic Prepared upon Field‐Assisted Sintering Technique/Spark Plasma Sinteringcitations
- 2024Dealing with Missing Angular Sections in NanoCT Reconstructions of Low Contrast Polymeric Samples Employing a Mechanical In Situ Loading Stage
- 2024The effect of grain boundaries and precipitates on the mechanical behavior of the refractory compositionally complex alloy NbMoCrTiAlcitations
- 2023Dealing with missing angular sections in nanoCT reconstructions of low contrast polymeric samples employing a mechanical in situ loading stage
- 20233D‐Printed Inherently Porous Structures with Tetrahedral Lattice Architecture: Experimental and Computational Study of Their Mechanical Behavior
- 2022Lab-based in situ nanoCT as a tool for the 3D structural and mechanical characterization of metamaterials
- 2021Architectural tunability of mechanical metamaterials in the nanometer rangecitations
- 2021Controlling shear band instability by nanoscale heterogeneities in metallic nanoglassescitations
- 2021Optimization of sintering conditions for improved microstructural and mechanical properties of dense Ce0.8Gd0.2O2-δ-FeCo2O4 oxygen transport membranescitations
- 2020Dislocation structures and the role of grain boundaries in cyclically deformed Ni micropillarscitations
- 2020Nanoscale patterning at the Si/SiO<sub>2</sub>/graphene interface by focused He<sup>+</sup> beamcitations
- 2019Size Effect on the Strength and Deformation Behavior of Glassy Carbon Nanopillars
- 2019Sliding wear behavior of fully nanotwinned Cu alloys
- 2018Micromechanics-based investigation of the elastic properties of polymer-modified cementitious materials using nanoindentation and semi-analytical modelingcitations
- 2017Annealing-induced recovery of indents in thin Au(Fe) bilayer films
- 2017Micromechanical study on the deformation behavior of directionally solidified NiAl–Cr eutectic compositescitations
- 2017Micromechanics-based prediction of the elastic properties of polymer-modified cementitious materials
- 2016Hydration of magnesia cubes: a helium ion microscopy study
- 2016Deformation mechanisms and morphology of metallic multilayers revealed by nanosliding and nanoindentation
- 2006Size effects on deformation and fracture of nanostructured metalscitations
Places of action
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article
Optimization of sintering conditions for improved microstructural and mechanical properties of dense Ce0.8Gd0.2O2-δ-FeCo2O4 oxygen transport membranes
Abstract
<p>Ce<sub>0.8</sub>Gd<sub>0.2</sub>O<sub>2-</sub><sub>δ</sub>-FeCo<sub>2</sub>O<sub>4</sub> composite is an excellent oxygen transport membrane material with good chemical stability for applications in oxygen separation and membrane reactors. To improve microstructural and mechanical properties, sintering profiles for Ce<sub>0.8</sub>Gd<sub>0.2</sub>O<sub>2-</sub><sub>δ</sub>-FeCo<sub>2</sub>O<sub>4</sub> composites were optimized. Different sintering temperatures are selected based on our study of phase interactions among the initial powder mixtures using high-temperature X-ray diffraction. The results reveal that the phase interaction at ∼1050 ℃ accelerates densification process, and a further increase of sintering temperature to 1200 ℃ contributes to the homogenization of the pore distribution. A higher density and an improved homogeneity of pore distribution result in enhanced mechanical strength. However, the density decreases once the sintering temperature reaches 1350 ℃. Hence, the optimal sintering temperature considering both microstructural and mechanical properties appears to be 1200 ℃. Sintering at this temperature results in a microstructure with a density exceeding 99 % with only small surface defects and a high average flexural strength of approximately 266 MPa.</p>