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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Smith, W.
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Publications (5/5 displayed)
- 2023Towards aerospace grade thin-ply composites ::effect of ply thickness, fibre, matrix and interlayer toughening on strength and damage tolerancecitations
- 2023Thin ply composites ::experimental characterization and modeling of size-effectscitations
- 2016Global research alliance on agricultural greenhouse gases - benchmark and ensemble crop and grassland model estimates
- 2014A novel approach for the preparation of textured CuO thin films from electrodeposited CuCl and CuBrcitations
- 2006Sample preparation for nanoanalytical electron microscopy using the FIB lift-out method and low energy ion millingcitations
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article
A novel approach for the preparation of textured CuO thin films from electrodeposited CuCl and CuBr
Abstract
We report on the electrodeposition of CuX (X = Cl, Br) thin films on fluorine-doped tin oxide (FTO) electrodes. The electrodeposited CuX thin films, for the first time, were used as intermediates to prepare CuO thin films. Calcination of the as-prepared CuX thin films at temperatures above 380 C allowed us to produce CuO thin films, which were used in photoelectrochemical (PEC) studies. The highest recorded photocurrent density of ∼1.3 mA/cm <sup>2</sup> at -0.55 V (vs. Ag/AgCl) in aqueous solution was obtained from the CuO sample calcined at 460 C. Here, we showed that the photocurrent in the unprotected CuO electrode originates from corrosion, formation of Cu <sub>2</sub>O and Cu phases, and not from water-splitting process as it has been claimed in literature. In addition, the electrochemical impedance spectroscopy allowed us to obtain the flat-band potentials of the CuO films. © 2014 Elsevier B.V. All rights reserved.