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| Naji, M. |
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| Azam, Siraj |
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| Azevedo, Nuno Monteiro |
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Louhi-Kultanen, Marjatta
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Publications (4/4 displayed)
- 2020Freeze Concentration of Aqueous [DBNH][OAc] Ionic Liquid Solutioncitations
- 2016Pulsed electric field assisted sol–gel preparation of TiO2nanoparticlescitations
- 2014Growth and characterization of 6-chloro-2,4-dinitroaniline crystals in anti-solvent precipitation and reprecipitation methodscitations
- 2005IR spectroscopy together with multivariate data analysis as a process analytical tool for in-line monitoring of crystallization process and solid-state analysis of crystalline productcitations
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article
Pulsed electric field assisted sol–gel preparation of TiO2nanoparticles
Abstract
<p>This work studies the effect of a pulsed electric field (PEF) on the precipitation and properties of TiO<sub>2</sub>nanoparticles. TiO<sub>2</sub>nanoparticles were prepared using pulsed DC electric field assisted sol–gel method. The duration of the PEF treatment was varied to investigate its effect on the particle size of TiO<sub>2</sub>nanoparticles. The nanoparticles were characterized by X-ray powder diffraction (XRD), Raman spectroscopy, UV diffuse reflectance spectroscopy (UV-DRS) and transmission electron microscopy (TEM). It was found that TiO<sub>2</sub>particles prepared with pulsed electric field assisted sol-gel method had enhanced average crystallite size due to the effect of the pulsed electric field on primary nucleation. The effect of electric field on nanoparticle preparation is interesting which can be used to control the grain and crystallite size of nanoparticle.</p>