Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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Lancaster University

in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (11/11 displayed)

  • 2022Synthesis of green thermo-responsive amphoteric terpolymer functionalized silica nanocomposite derived from waste vegetable oil triglycerides for enhanced oil recovery (EOR)11citations
  • 2019Synthesis and characterization of a novel amphoteric terpolymer nanocomposite for enhanced oil recovery applicationscitations
  • 2019Synthesis and characterization of a novel amphoteric terpolymer nanocomposite for enhanced oil recovery applicationscitations
  • 2019Systematic multivariate optimisation of butylene carbonate synthesis via CO <inf>2</inf> utilisation using graphene-inorganic nanocomposite catalysts12citations
  • 2018Greener synthesis of dimethyl carbonate using a novel tin-zirconia/graphene nanocomposite catalyst55citations
  • 2018A facile and greener synthesis of butylene carbonate via CO2 utilisation using a novel copper–zirconia oxide/graphene catalystcitations
  • 2018Greener synthesis of butylene carbonate via CO2 utilisation using graphene-inorganic nanocomposite catalystscitations
  • 2018Greener synthesis of 1,2-butylene carbonate from CO2 using graphene-inorganic nanocomposite catalyst15citations
  • 2017Greener synthesis of styrene carbonate from CO2 using graphene-inorganic nanocomposite catalystscitations
  • 2017Greener synthesis of 1, 2 butylene carbonate from CO2 using graphene-inorganic nanocomposite catalysiscitations
  • 2017Carbon dioxide utilization by graphene based nanocomposite materials as catalystscitations

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Attia, Attia
1 / 1 shared
Mahran, Shahenda
2 / 2 shared
Zadeh, Z.
1 / 1 shared
Attia, A.
1 / 2 shared
Mahran, S.
1 / 1 shared
Echresh Zadeh, Zahra
1 / 1 shared
Attia, Attia M.
1 / 1 shared
Aboelazayem, O.
3 / 3 shared
Onyenkeadi, V.
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Heil, Tobias
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Morgan, David
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Kellici, Suela
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Lampronti, Giulio I.
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Saada, Rim
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Aboelazayem, Omar
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2019
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Co-Authors (by relevance)

  • Attia, Attia
  • Mahran, Shahenda
  • Zadeh, Z.
  • Attia, A.
  • Mahran, S.
  • Echresh Zadeh, Zahra
  • Attia, Attia M.
  • Aboelazayem, O.
  • Onyenkeadi, V.
  • Heil, Tobias
  • Morgan, David
  • Kellici, Suela
  • Lampronti, Giulio I.
  • Saada, Rim
  • Aboelazayem, Omar
OrganizationsLocationPeople

article

Synthesis of green thermo-responsive amphoteric terpolymer functionalized silica nanocomposite derived from waste vegetable oil triglycerides for enhanced oil recovery (EOR)

  • Saha, Basudeb
  • Attia, Attia
  • Mahran, Shahenda
Abstract

Despite the high efficiency of polymer flooding as a chemical enhanced oil recovery (CEOR) technique, the low thermal stability and poor salt resistance of widely applied partially hydrolyzed polyacrylamide (HPAM) limited the application of this technique in oil reservoirs at harsh reservoir conditions of high–temperature and high–salinity (HTHS). These inadequacies of HPAM, result in the urge for an environmentally friendly polymer with good viscosifying properties and a substantial effect on mobility ratio at HTHS reservoir conditions. In this research, a high oleic acid waste vegetable oil (WVO) is utilized to synthesize a novel environmentally benign, thermo-responsive amphoteric nanocomposite for EOR applications at HTHS reservoir conditions. A green route transesterification reaction has been utilized to synthesize a novel thermo-sensitive monomer from WVO. The existence of unsaturated fatty acids isolated double bonds and acryloyl functional groups in the synthesized monomer has been confirmed using different characterization methods. The reactive acryloyl double bond in the synthesized monomer has been copolymerized with acrylamide, acrylacyloxyethyltrimethyl ammonium chloride, and 2-acrylamide-2-methylpropane sulfonic acid in presence of dimethylphenylvinylsilane via free radical emulsion polymerization. The synthesized nanocomposite has been characterized by FTIR, 1H NMR, SEM, EDX, TEM, and DLS. The thermal stability of the nanocomposite has been evaluated by TGA and DTA analysis. The results indicated that nanocomposite solution exhibited a pouncing thermo-thickening behaviour and superior viscosifying properties even at an ultra-low polymer concentration of 0.04 wt.% as the temperature increased from 25 to 100 °C, with increasing salinity from 10,000 to 230,000 ppm as well as salt-free solutions. Flooding experiments demonstrated that the oil recovery factor reached 15.4 ± 0.1% using low nanocomposite concentrations of 0.04 wt.%, 22.6 ± 0.3% using nanocomposite concentrations of 0.06 wt.% and 25 ± 0.2% using 0.1 wt.% nanocomposite concentrations evaluated under hostile conditions of 100 °C and salinity of about 230,000 ppm. This research offers a new direction for the synthesis of a novel green, high molecular weight thermo-responsive nanocomposite for EOR application at extremely harsh reservoir conditions via WVO valorization.

Topics
  • nanocomposite
  • impedance spectroscopy
  • polymer
  • mobility
  • scanning electron microscopy
  • experiment
  • reactive
  • transmission electron microscopy
  • thermogravimetry
  • Energy-dispersive X-ray spectroscopy
  • molecular weight
  • Nuclear Magnetic Resonance spectroscopy
  • differential thermal analysis
  • dynamic light scattering