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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Sastry, Murali
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (7/7 displayed)
- 2012Ultra-low level optical detection of mercuric ions using biogenic gold nanotrianglescitations
- 2004Phase transfer of platinum nanoparticles from aqueous to organic solutions using fatty amine moleculescitations
- 2004Use of aqueous foams for the synthesis of gold nanoparticles of variable morphologycitations
- 2004A low-temperature, soft chemistry method for the synthesis of zirconia nanoparticles in thermally evaporated fatty amine thin filmscitations
- 2004One-step synthesis of ordered two-dimensional assemblies of silver nanoparticles by the spontaneous reduction of silver ions by pentadecylphenol langmuir monolayerscitations
- 2004Variation in morphology of gold nanoparticles synthesized by the spontaneous reduction of aqueous chloroaurate ions by alkylated tyrosine at a liquid-liquid and air-water interfacecitations
- 2003Assembling gold nanoparticles in solution using phosphorothioate DNA as structural interconnects
Places of action
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article
A low-temperature, soft chemistry method for the synthesis of zirconia nanoparticles in thermally evaporated fatty amine thin films
Abstract
<p>We demonstrate the synthesis of zirconia nanoparticles in a lipid matrix by a simple, low temperature beaker-based process. This is accomplished by electrostatic entrapment of ZrF<sub>6</sub><sup>2-</sup> ions within thermally evaporated octadecylamine (ODA) thin films followed by the low-temperature in situ hydrolysis of the entrapped metal ion complexes. The zirconia particles thus formed were of the monoclinic phase and were fairly monodisperse with particles of average size 40 nm. The zirconia crystallites appeared to exhibit preferred orientation indicating epitaxial growth of the crystals within the lipid matrix. The formation of zirconia nanoparticles in the lipid matrix was investigated using quartz crystal microgravimetry (QCM), optical absorption spectroscopy, X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM), and X-ray diffraction (XRD) techniques.</p>