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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Vanpoucke, Danny E. P.
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Topics
Publications (8/8 displayed)
- 2024Extreme Machine Learning: When the average model knows best
- 2021Impact of methane concentration on surface morphology and boron incorporation of heavily boron-doped single crystal diamond layerscitations
- 2020Investigation of structural, electronic and magnetic properties of breathing metal-organic framework MIL-47(Mn): a first principles approachcitations
- 2020Investigation of structural, electronic and magnetic properties of breathing metal-organic framework MIL-47(Mn)citations
- 2019Synthesis, characterization and thermodynamic stability of nanostructured ε-iron carbonitride powder prepared by a solid-state mechanochemical routecitations
- 2017A combined experimental and theoretical investigation of the Al-Melamine reactive milling systemcitations
- 2016Mechanochemical route to the synthesis of nanostructured Aluminium nitridecitations
- 2013New Functionalized Metal-Organic Frameworks MIL-47-X (X = -Cl, -Br, -CH3, -CF3, -OH, -OCH3)citations
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article
A combined experimental and theoretical investigation of the Al-Melamine reactive milling system
Abstract
<p>A versatile ball milling process was employed for the synthesis of hexagonal aluminum nitride (h-AlN) through the reaction of metallic aluminum with melamine. A combined experimental and theoretical study was carried out to evaluate the synthesized products. Milling intermediates and products were fully characterized via various techniques including XRD, FTIR, XPS, Raman and TEM. Moreover, a Boltzmann distribution model was proposed to investigate the effect of milling energy and reactant ratios on the thermodynamic stability and the proportion of different milling products. According to the results, the reaction mechanism and milling products were significantly influenced by the reactant ratio. The optimized condition for AlN synthesis was found to be at Al/M molar ratio of 6, where the final products were consisted of nanostructured AlN with average crystallite size of 11 nm and non-crystalline heterogeneous carbon. (C) 2017 Elsevier B.V. All rights reserved.</p>