| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Mitterer, Christian
Montanuniversität Leoben
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (28/28 displayed)
- 2024Enhancement of copper nanoparticle yield in magnetron sputter inert gas condensation by applying substrate bias voltage and its influence on thin film morphologycitations
- 2024Short-Time Magnetron Sputtering for the Development of Carbon–Palladium Nanocomposites
- 2023Improved thermolytic dehydrogenation of LiBH4 nanoconfined in few-layer graphene with different functionalitiescitations
- 2023Parameters influencing the fracture of Mo films and their wider significancecitations
- 2023Synergistic enhancement of hydrogen interactions in palladium–silicon–gold metallic glass with multilayered graphenecitations
- 2023Synergistic enhancement of hydrogen interactions in palladium-gold-silicon metallic glass on multilayered graphenecitations
- 2022Impact of Si on the high-temperature oxidation of AlCr(Si)N coatingscitations
- 2022Determination of Cooling Rate and Temperature Gradient during Formation of Cathode Spot Craters in a Vacuum Arccitations
- 2022Magnetron Sputtered Non‐Toxic and Precious Element‐Free TiZrGe Metallic Glass Nanofilms with Enhanced Biocorrosion Resistancecitations
- 2022Precipitation-based grain boundary design alters Inter- to Trans-granular Fracture in AlCrN Thin Filmscitations
- 2021Rapid solidification and metastable phase formation during surface modifications of composite Al-Cr cathodes exposed to cathodic arc plasmacitations
- 2021Synthesis of bulk reactive Ni–Al composites using high pressure torsioncitations
- 2020Effect of Pt nanoparticle decoration on the H2 storage performance of plasma-derived nanoporous graphenecitations
- 2020Influence of spinodal decomposition and fcc→w phase transformation on global and local mechanical properties of nanolamellar CVD fcc-Ti1-xAlxN coatingscitations
- 2020Stress relaxation through thermal crack formation in CVD TiCN coatings grown on WC-Co with different Co contentscitations
- 2020Nanoscale stress distributions and microstructural changes at scratch track cross-sections of a deformed brittle-ductile CrN-Cr bilayercitations
- 2020Evolution of stress fields during crack growth and arrest in a brittle-ductile CrN-Cr clamped-cantilever analysed by X-ray nanodiffraction and modellingcitations
- 2019Anisotropy of fracture toughness in nanostructured ceramics controlled by grain boundary designcitations
- 2019Thermal stability of nanolamellar fcc-Ti1-xAlxN grown by chemical vapor depositioncitations
- 2019Stress-controlled decomposition routes in cubic AlCrN films assessed by in-situ high-temperature high-energy grazing incidence transmission X-ray diffractioncitations
- 2018Novel combustion synthesis of carbon foam‑aluminum fluoride nanocomposite materialscitations
- 2018Needle grass array of nanostructured nickel cobalt sulfide electrode for clean energy generationcitations
- 2017Solvothermal synthesis, nanostructural characterization and gas cryo-adsorption studies in a metal-organic framework (IRMOF-1) materialcitations
- 2016In-situ Observation of Cross-Sectional Microstructural Changes and Stress Distributions in Fracturing TiN Thin Film during Nanoindentationcitations
- 2016Hierarchical Architectures to Enhance Structural and Functional Properties of Brittle Materialscitations
- 2016Cross-sectional structure-property relationship in a graded nanocrystalline Ti1-xAlxN thin filmcitations
- 2014Mono-textured nanocrystalline thin films with pronounced stress-gradientscitations
- 2007Tribological properties of nanocomposite CrC x /a-C:H thin filmscitations
Places of action
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article
Solvothermal synthesis, nanostructural characterization and gas cryo-adsorption studies in a metal-organic framework (IRMOF-1) material
Abstract
A nanoporous metal–organic framework material, exhibiting an IRMOF-1 type crystalline structure, was prepared by following a direct solvothermal synthesis approach, using zinc nitrate and terephthalic acid as precursors and dimethylformamide as solvent, combined with supercritical CO2 activation and vacuum outgassing procedures. A series of advanced characterization methods were employed, including scanning electron microscopy, Fourier-transform infrared radiation spectroscopy and X-ray diffraction, in order to study the morphology, surface chemistry and structure of the IRMOF-1 material directly upon its synthesis. Porosity properties, such as Brunauer–Emmet–Teller (BET) specific area (∼520 m2/g) and micropore volume (∼0.2 cm3/g), were calculated for the activated sample based on N2 gas sorption data collected at 77 K. The H2 storage performance was preliminary assessed by low-pressure (0–1 bar) H2 gas adsorption and desorption measurements at 77 K. The activated IRMOF-1 material of this study demonstrated a fully reversible H2 sorption behavior combined with an adequate gravimetric H2 uptake relative to its BET specific area, thus achieving a value of ∼1 wt.% under close-to-atmospheric pressure conditions.