| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Escudero-Escribano, María
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (10/10 displayed)
- 2024Toward understanding CO oxidation on high-entropy alloy electrocatalystscitations
- 2024Preparation and characterization of bimetallic and multimetallic nanostructured materials for electrocatalysis
- 2024Composition effects of electrodeposited Cu-Ag nanostructured electrocatalysts for CO2 reductioncitations
- 2024Composition effects of electrodeposited Cu-Ag nanostructured electrocatalysts for CO 2 reductioncitations
- 2024Preparation of Tunable Cu−Ag Nanostructures by Electrodeposition in a Deep Eutectic Solventcitations
- 2023Nanostructured Ir-based electrocatalysts for oxygen evolution prepared by galvanic displacement of Co and Nicitations
- 2022Surfactant-free syntheses and pair distribution function analysis of osmium nanoparticlescitations
- 2022Pd-Au Nanostructured Electrocatalysts with Tunable Compositions for Formic Acid Oxidationcitations
- 2022Pd-Au Nanostructured Electrocatalysts with Tunable Compositions for Formic Acid Oxidationcitations
- 2021Preparation of high surface area Cu-Au bimetallic nanostructured materials by co-electrodeposition in a deep eutectic solventcitations
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article
Preparation of high surface area Cu-Au bimetallic nanostructured materials by co-electrodeposition in a deep eutectic solvent
Abstract
Our sustainable future requires finding new, affordable and green routes to prepare nanostructured materials used in renewable energy conversion. In this work we present an electrodeposition method in a deep eutectic solvent (DES) to prepare bimetallic high surface area nanostructures of Cu and Au with tunable structure and composition. The metal electrodeposition performed in choline chloride within a urea deep eutectic solvent allows us to tailor the size, morphology and elemental composition of the deposits. We combine electrochemical methods with scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and energy dispersive X-ray spectroscopy (EDS) to characterize the electrodeposited nanostructured materials. We assess the increase of the electroactive surface area through the analysis of the lead underpotential deposition (UPD) on the prepared films. Integrated Pb UPD charge values of ca. 1600–4000 μC/cm 2 for the prepared Cu-Au films have been calculated, suggesting a 5–14 fold increase of the active surface area compared to flat surfaces of polycrystalline Cu or Au. Our work reports a versatile and environmentally friendly route for the electrodeposition of Cu-Au bimetallic nanostructures in a DES. The combination of a tailored morphology and composition with the high active surface area of the nanostructured materials show that electrodeposition in DES is promising for the development of multimetallic electrocatalysts.