| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Pardanaud, Cedric
French National Centre for Scientific Research
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2022The role of defects, deuterium, and surface morphology on the optical response of berylliumcitations
- 2019Investigating the possible origin of Raman bands in defective sp2/sp3 carbons below 900 cm−1: Phonon density of states or double resonance mechanism at play?citations
- 2017Raman Microscopy : a Suitable Tool For Characterizing Surfaces in interaction With Plasmas in The Field of Nuclear Fusioncitations
- 2015In-plane and out-of-plane defects of graphite bombarded by H, D and He investigated by atomic force and Raman microscopiescitations
- 2014Multiwavelength Raman spectroscopy analysis of a large sampling of disordered carbons extracted from the Tore Supra tokamakcitations
- 2013Raman spectroscopy investigation of the H content of heated hard amorphous carbon layerscitations
- 2013Long Term H-Release from Amorphous Carbon Evidenced by in Situ Raman Microscopy under Isothermal Heatingcitations
- 2012Raman micro-spectroscopy as a tool to measure the absorption coefficient and the erosion rate of hydrogenated amorphous carbon films heat-treated under hydrogen bombardmentcitations
- 2011Raman study of CFC tiles extracted from the toroidal pump limiter of Tore Supracitations
Places of action
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article
Long Term H-Release from Amorphous Carbon Evidenced by in Situ Raman Microscopy under Isothermal Heating
Abstract
We study the kinetics of the H release from plasma-deposited hydrogenated amorphous carbon films under isothermal heating at 450, 500 and 600 °C for long times up to several days using in situ Raman microscopy. Four Raman parameters are analyzed. They allow the identification of different processes such as the carbon network reorganization and the H release from sp3 or sp2 carbon atoms and the corresponding timescales. Carbon reorganization with aromatization and loss of sp3 hybridization occurs first in 100 minutes at 500 °C. The final organization is similar at all investigated temperatures. Full H release from sp3 carbon occurs on a longer timescale of about 10 hours while H release from sp2 carbon atoms is only partial, even after several days. All these processes occur more rapidly with higher initial H content, in agreement with what is known about the stability of these types of films. A quantitative analysis of these kinetics studies gives valuable information about the microscopic processes at the origin of the H release through the determination of activation energies.