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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Ginjeira, António
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Publications (7/7 displayed)
- 2022In Situ Zymography Analysis of Matrix Metalloproteinases Activity Following Endodontic Irrigation Protocols and Correlation to Root Dentine Bond Strengthcitations
- 2022Comparison of five rotary systems regarding design, metallurgy, mechanical performance, and canal preparation—a multimethod researchcitations
- 2022Multimethod Assessment of Design, Metallurgical, and Mechanical Characteristics of Original and Counterfeit ProGlider Instrumentscitations
- 2021Effect of different manipulations on the physical, chemical and microstructural characteristics of Biodentinecitations
- 2021A survey on root canal obturation trends: warm versus cold obturation technique
- 2020Influence of Kinematics on the Cyclic Fatigue Resistance of Replicalike and Original Brand Rotary Instrumentscitations
- 2017Fatigue resistance of rotary endodontic files subjected to planar and non-planar curvatures induced by in vitro tooth canalscitations
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article
Effect of different manipulations on the physical, chemical and microstructural characteristics of Biodentine
Abstract
Objective<br/>The water to powder ratio and method of mixing is important for the properties of hydraulic cements. For this purpose a number of clinicians prefer premixed materials. Dental manufacturing companies provide predosed materials, however the manufacturer instructions are not always adhered to. The aim of this research is to investigate physical and chemical alterations of the tricalcium silicate‐based cement Biodentine when manipulated according to the manufacturer’s instructions (control) or changing the doses and mixing of the material components.<br/><br/>Methods<br/>6 groups were constituted according to different mixing and dosing of powder and liquid. The hydrated cements were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR). Calcium ion concentration of the leachate was also investigated. Assessment of the physical characteristics included setting time and microhardness.<br/><br/>Results<br/>Microstructural differences were visible only in the Biodentine mixed manually with water, in which early hydration rate was also affected, with lower calcium ion release. Increase of Biodentine liquid increased the calcium ion release, but also increased the setting time. Manual manipulation required more liquid (both water and Biodentine liquid) added to the mixture to guarantee a similar consistency to the control. A decrease in setting time was also noted. All groups showed higher values of microhardness at 24 h compared to the freshly set materials. In the freshly set materials, there was an overall decrease in microhardness in all groups when compared to group control, particularly significant when increasing the dosage of Biodentine liquid.<br/><br/>Significance<br/>When mixing Biodentine, altering the mixing procedure in terms of type and amount of liquid added to the powder and mixing device chosen has an effect on the physical, chemical and mechanical characteristics and surface topography of the material, when compared to Biodentine mixed according to the manufacturer’s recommendations. Hence, the manufacturer’s instructions should be strictly followed.