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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Chen, Xiaohui
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (22/22 displayed)
- 2022Effect of sandblasting with fluorapatite glass-ceramic powder and chemical primers/adhesives on shear bond strength of indirect repairing composite to zirconiacitations
- 2020Fluorapatite Glass-Ceramics: A New Sandblasting Approach for Zirconia Repair
- 2019Preliminary study of hydroxyapatite particles air abrasive blasting on Mg-4Zn-0.3Ca surfacecitations
- 2016Design and Synthesis of New Translucent, High Strength Leucite Glass-Ceramics
- 2016Surface properties of tricalcium phosphate and hydroxyapatite resin composites
- 2014Leucite Glass Ceramics
- 2014The Retarding Effect of Zinc Oxide on Dissolution and Apatite Formation of a Fluoride Containing Bioactive Glass
- 2014'Smart' acid-degradable zinc-releasing silicate glassescitations
- 2014Low-sodium Bioactive Glass Coatings for Titanium Implants by Grit Blasting
- 2013Remineralisation Study of a Nano-sized Hydroxyapatite and Fluoride Containing Toothpaste
- 2013Reduced wear of enamel with novel fine and nano-scale leucite glass-ceramicscitations
- 2013Crystallization of high-strength nano-scale leucite glass-ceramicscitations
- 2012Wear characteristics of fine and nano-scale high-strength leucite glass-ceramics
- 2011Crystallization and flexural strength optimization of fine-grained leucite glass-ceramics for dentistrycitations
- 2010Development and testing of multi-phase glazes for adhesive bonding to zirconia substrates
- 2010Crystallization of high-strength fine-sized leucite glass-ceramicscitations
- 2010Synthesis of nano-sized Leucite Glass-ceramics
- 2010Wear Characteristics of an Experimental High-Strength Fine-Sized Leucite Glass-Ceramic
- 2010Optimization of Novel Leucite Glass-ceramics
- 2009Effect of Glass Powder Size on Leucite Glass-Ceramic Crystallisation
- 2009Control of ceramic microstructure
- 2007Microstructure and Thermal Expansion Properties of Some Leucite Glass-Ceramics
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article
Crystallization and flexural strength optimization of fine-grained leucite glass-ceramics for dentistry
Abstract
Objectives: Leucite glass-ceramics with fine-grained leucite crystals promote improved mechanical strength and increased translucency. The objectives of the study were to optimize the microstructure of a fine-grained leucite glass-ceramic in order to increase its flexural strength and reliability as measured by its Weibull modulus. Methods: Glass was prepared by a melt-derived method and ground into a powder (M1A). The glass crystallization kinetics were investigated using high temperature XRD and DSC. A series of two-step heat treatments with different nucleation/crystal growth temperatures and holds were carried out to establish the optimized crystallization heat treatment. Glass-ceramics were characterized using XRD, SEM and dilatometry. The glass-ceramic heat treated at the optimized crystallization parameters (M1A opt) was both sintered (SM1Aopt) and heat extruded (EM1Aopt) into discs and tested using the biaxial flexural strength (BFS) test. Results: High temperature XRD suggested leucite and sanidine crystallization at different temperatures. Optimized crystallization resulted in an even distribution of fine leucite crystals (0.15 (0.09) μm2) in the glassy matrix, with no signs of microcracking. Glass-ceramic M1A opt showed BFS values of [mean (SD), MPa]: SM1Aopt = 252.4 (38.7); and EM1Aopt = 245.0 (24.3). Weibull results were: SM1A opt; m = 8.7 (C.I. = 7.5-10.1) and EM1Aopt; m = 11.9 (C.I. = 9.3-15.1). Both experimental groups had a significantly higher BFS and characteristic strength than the IPS Empress Esthetic glass-ceramic, with a higher m value for the EM1Aopt material (p <0.05). Significance: A processable fine-grained leucite glass-ceramic with high flexural strength and improved reliability was the outcome of this study. © 2011 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.