| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Bodner, Sabine C.
Montanuniversität Leoben
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (11/11 displayed)
- 2023Influence of Hatch Strategy on Crystallographic Texture Evolution, Mechanical Anisotropy of Laser Beam Powder Bed Fused S316L Steelcitations
- 2022Graded Inconel-stainless steel multi-material structure by inter- and intralayer variation of metal alloyscitations
- 2022Degradation of regenerated cellulose filaments by hydrogen chloride under aqueous and non-aqueous conditionscitations
- 2022Cracking mechanism in a laser powder bed fused cold-work tool steelcitations
- 2022Effect of cold deformation on the stress corrosion cracking resistance of a high-strength stainless steelcitations
- 2022Local microstructural evolution and the role of residual stresses in the phase stability of a laser powder bed fused cold-work tool steelcitations
- 2021Zerstörungsfreie Charakterisierung von Furnieren für strukturelle Verbundwerkstoffe
- 2021Correlative cross-sectional characterization of nitrided, carburized and shot-peened steelscitations
- 2021Predicting strength of Finnish birch veneers based on three different failure criteriacitations
- 2019Cross-sectional gradients of residual stresses, microstructure and phases in a nitrided steel revealed by 20 µm synchrotron X-ray diffraction
- 2018Combinatorial study of process parameters, microstructure and mechanical properties in Inconel 718 parts produced by additive manufacturing
Places of action
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article
Degradation of regenerated cellulose filaments by hydrogen chloride under aqueous and non-aqueous conditions
Abstract
Cellulose (rayon) filaments were exposed to various concentrations of hydrochloric acid under aqueous and non-aqueous conditions in order to study differences in degradation. Two sources of polymeric diphenylmethane diisocyanate (pMDI) were used as non-aqueous media. As a consequence of the production process, pMDI was found to contain residual hydrochloric acid. Filament yarns were immersed for either 7 h or 7 d and purified to obtain pure filaments for further analysis. Single-filament tensile tests and molar mass measurements confirmed a significant degradation of the filament structure under non-aqueous conditions. Samples with the same amount of hydrochloric acid immersed in water, however, were rarely affected. Complementary X-ray diffraction indicated that the removal of the amorphous cellulose resulted in an increase in the cellulose crystallinity, which was manifested by a decrease in the width of the diffraction peaks. With this remarkable difference between aqueous and non-aqueous treatments, a quantitative proof to a new aspect about the processability of regenerated cellulose was presented. Amongst other fields of technical applications, these findings will have to be considered in composite engineering dealing with cellulosic fibre reinforcements. An effective way to avoid acidic hydrolysis was presented based on calcium carbonate as matrix filler.