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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Ribitsch, Volker
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Topics
Publications (17/17 displayed)
- 2018Optimization of the Catalyst and Membrane Performance by addition of various Additives for the alkaline Direct Ethanol Fuel Cell
- 2015Cellulose thin films from ionic liquid solutions
- 2013Functional patterning of biopolymer thin films using enzymes and lithographic methodscitations
- 2013Chitosan-Silane Sol-Gel Hybrid Thin Films with controllable Layer Thickness and Morphologycitations
- 2013Comparison study of TEMPO and phthalimide-N-oxyl (PINO) radicals on oxidation efficiency toward cellulosecitations
- 2013Chemical modification and characterization of poly(ethylene terephthalate) surfaces for collagen immobilizationcitations
- 2012Adsorption of carboxymethyl cellulose on polymer surfacescitations
- 2011Wettability and surface composition of partly and fully regenerated cellulose thin films from trimethylsilyl cellulosecitations
- 2011Deposition of silicon doped and pure hydrogenated amorphous carbon coatings on quartz crystal microbalance sensors for protein adsorption studiescitations
- 2009Electrokinetic properties of polypropylene-layered silicate Nanocomposite fiberscitations
- 2008Adsorption of chitosan on PET films monitored by quartz crystal microbalancecitations
- 2005Determination of the accessible carboxyl and amino end groups in structurally modified PA 6 using titration methods
- 2004Determination of dissociable groups in natural and regenerated cellulose fibers by different titration methodscitations
- 2004Determining the Surface Free Energy of Cellulose Materials with the Powder Contact Angle Methodcitations
- 2003Characterisation of modified polypropylene fibrescitations
- 2002Modifikacije PA 6 z NH3 plazmo
- 2000Analiza povrsine vlaken z mikroskopijo atomskih sil (AFM)
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article
Chitosan-Silane Sol-Gel Hybrid Thin Films with controllable Layer Thickness and Morphology
Abstract
The preparation of thin films of chitosan–silane hybrid materials by combining sol–gel processing and spin coating is reported. A variety of silanes can be used as starting materials for the preparation of such thin films, namely tetraethoxysilane, tri-tert-butoxysilanol, trimethylethoxysilane, p-trifluoromethyltetra-fluorophenyltriethoxysilane, trivinylmethoxysilane, (methoxymethyl)trimethyl-silane, and hexamethoxydisilane. These silanes are subjected to a sol–gel process before they are added to acidic chitosan solutions. The chitosan:silane ratio is kept constant at 6:1 (w/w) and dilutions with ethanol are prepared and spin coated. Depending on the degree of dilution, film thickness can be controlled in a range between 5 and 70 nm. For the determination of additional surface properties, static water contact angle measurements and atomic force microscopy have been employed.