Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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in Cooperation with on an Cooperation-Score of 37%

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Publications (7/7 displayed)

  • 2020In vitro assessment of polyethylene glycol and polyvinylpyrrolidone as hydrophilic additives on bioseparation by polysulfone membranes13citations
  • 2017Synthesis of distinctly thiol-capped CdTe quantum dots under microwave heating: multivariate optimization and characterization27citations
  • 2011Novel LTCC-potentiometric microfluidic device for biparametric analysis of organic compounds carrying plastic antibodies as ionophores: Application to sulfamethoxazole and trimethoprim32citations
  • 2009Modeling, Structural, and Spectroscopic Studies of Lanthanide-Organic Frameworks64citations
  • 2006Extraction and recovery of chromium from electroplating sludge87citations
  • 2003Monosegemented flow potentiometric titration for the determination of chloride in milk and wine13citations
  • 2001Sequential injection analysis of captopril based on colorimetric and potentiometric detection52citations

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Araujo, Ad
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Solich, P.
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Amorim, Cg
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Santos Silva, A.
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Kohlova, M.
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Araujo, An
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Araujo, Nn
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Pimenta, Am
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Co-Authors (by relevance)

  • Araujo, Ad
  • Solich, P.
  • Amorim, Cg
  • Santos Silva, A.
  • Kohlova, M.
  • Araujo, An
  • Rodrigues, Ssm
  • Soares, Jx
  • Melo, A.
  • Santos, Jlm
  • De Souza, Gcs
  • Ribeiro, Dsm
  • Alonso Chamarro, J.
  • Sales, Mgf
  • Arasa, E.
  • Almeida, Saa
  • Martinez Cisneros, Cs
  • Puyol, M.
  • Freire, Ro
  • Almeida Paz, Faa
  • Galembeck, A.
  • De Sa, Gf
  • Alves, S.
  • Rodrigues, Mo
  • Da Silva, Vl
  • Neto, Bd
  • Duarte, Mmm
  • De Mello, Nt
  • Silva, Ptd
  • Raimundo, Im
  • Vieira, Ja
  • Reis, Bf
  • Araujo, Nn
  • Pimenta, Am
OrganizationsLocationPeople

article

Novel LTCC-potentiometric microfluidic device for biparametric analysis of organic compounds carrying plastic antibodies as ionophores: Application to sulfamethoxazole and trimethoprim

  • Alonso Chamarro, J.
  • Montenegro, Mcbsm
  • Sales, Mgf
  • Arasa, E.
  • Almeida, Saa
  • Martinez Cisneros, Cs
  • Puyol, M.
Abstract

Monitoring organic environmental contaminants is of crucial importance to ensure public health. This requires simple, portable and robust devices to carry out on-site analysis. For this purpose, a low-temperature co-fired ceramics (LTCC) microfluidic potentiometric device (LTCC/mu POT) was developed for the first time for an organic compound: sulfamethoxazole (SMX). Sensory materials relied on newly designed plastic antibodies. Sol-gel, self-assembling monolayer and molecular-imprinting techniques were merged for this purpose. Silica beads were amine-modified and linked to SMX via glutaraldehyde modification. Condensation polymerization was conducted around SMX to fill the vacant spaces. SMX was removed after, leaving behind imprinted sites of complementary shape. The obtained particles were used as ionophores in plasticized PVC membranes. The most suitable membrane composition was selected in steady-state assays. Its suitability to flow analysis was verified in flow-injection studies with regular tubular electrodes. The LTCC/mu POT device integrated a bidimensional mixer, an embedded reference electrode based on Ag/AgCl and an Ag-based contact screen-printed under a micromachined cavity of 600 mu m depth. The sensing membranes were deposited over this contact and acted as indicating electrodes. Under optimum conditions, the SMX sensor displayed slopes of about -58.7 mV/decade in a range from 12.7 to 250 mu g/mL, providing a detection limit of 3.85 mu g/mL and a sampling throughput of 36 samples/h with a reagent consumption of 3.3 mL per sample. The system was adjusted later to multiple analyte detection by including a second potentiometric cell on the LTCC/mu POT device. No additional reference electrode was required. This concept was applied to Trimethoprim (TMP), always administered concomitantly with sulphonamide drugs, and tested in fish-farming waters. The biparametric microanalyzer displayed Nernstian behaviour, with average slopes -54.7 (SMX) and +57.8 (TMP) mV/decade. To demonstrate the microanalyzer capabilities for real applications, it was successfully applied to single and simultaneous determination of SMX and TMP in aquaculture waters.

Topics
  • impedance spectroscopy
  • compound
  • polymer
  • ceramic
  • amine
  • condensation polymerization