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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Dobkowska, Anna
Warsaw University of Technology
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (33/33 displayed)
- 2024Microstructure and Corrosion of Mg-Based Composites Produced from Custom-Made Powders of AZ31 and Ti6Al4V via Pulse Plasma Sinteringcitations
- 2024Microstructural, corrosion and mechanical properties of a WE43 alloycitations
- 2024Microstructural, corrosion and mechanical properties of a WE43 alloy: conventional extrusion versus SPDcitations
- 2023In vitro and in vivo degradation behavior of Mg-0.45Zn-0.45Ca (ZX00) screws for orthopedic applicationscitations
- 2023How to control the crystallization of metallic glasses during laser powder bed fusion? Towards part-specific 3D printing of in situ compositescitations
- 2023Microstructure and properties of an AZ61 alloy after extrusion with a forward-backward oscillating die without preheating of the initial billetcitations
- 2023In-depth analysis of the influence of bio-silica filler (Didymosphenia geminata frustules) on the properties of Mg matrix compositescitations
- 2022The Effect of Extrusion Ratio on the Corrosion Resistance of Ultrafine-Grained Mg-4Li-3Al-Zn Alloy Deformed Using Extrusion with a Forward-Backward Oscillating Diecitations
- 2022Microstructure and corrosion resistance characteristics of Ti–AlN composite produced by selective laser meltingcitations
- 2022Evolution of microstructure dependent corrosion properties of ultrafine AZ31 under conditions of extrusion with a forward backward oscillating diecitations
- 2022A comparison of the microstructure-dependent corrosion of dual-structured Mg-Li alloys fabricated by powder consolidation methods: Laser powder bed fusion vs pulse plasma sinteringcitations
- 2022The Role of LPSO Structures in Corrosion Resistance of Mg-Y-Zn Alloyscitations
- 2022Effect of annealing on the mechanical and corrosion properties of 316L stainless steel manufactured by laser powder bed fusioncitations
- 2022Corrosion behavior of fine-grained Mg-7.5Li-3Al-1Zn fabricated by extrusion with a forward-backward rotating die (KoBo)citations
- 2022How to Control the Crystallization of Metallic Glasses During Laser Powder Bed Fusion? Towards Part-Specific 3d Printing of in Situ Composites
- 2021Microstructure and corrosion resistance of a duplex structured Mg–7.5Li–3Al–1Zncitations
- 2021Influence of bimodal grain size distribution on the corrosion resistance of Mg–4Li–3Al–1Zn (LAZ431)citations
- 2021Biological and Corrosion Evaluation of In Situ Alloyed NiTi Fabricated through Laser Powder Bed Fusion (LPBF)citations
- 2020The Influence of Microstructure on Corrosion Resistance of Mg-3Al-1Zn-15Li (LAZ1531) Alloycitations
- 2020Nickel composite coatings reinforced nano SiC particles
- 2019The impact of different volume fractions of crystalline structures on the electrochemical behaviour of Mg67Zn29Ca4alloys for biomedical applicationscitations
- 2019The influence of Mg addition and hydrostatic extrusion HE on the repassivation ability of pure Al, AlMg1 and AlMg3 model alloys in 3.5 wt-% NaClcitations
- 2019Effect of Various Organic Additives in Galvanic Bath on Properties of Ni-SiC Composite Coatingscitations
- 2018Effect of structure on corrosion resistance of Mg-Zn-Ca alloy
- 2017Microstructure characterization of ceramic shell molds
- 2017Comparison of corrosion resistance of glass fiber reinforced composites and steels applicable for extraction pipes
- 2017The influence of grain refinement on the corrosion rate of carbon steels in fracturing fluids used in shale gas productioncitations
- 2016Analiza warstw korozyjnych w stalach wykorzystywanych w przemyśle wydobywczym po badaniach korozji naprężeniowej — Analysis of corrosive layers formed on the steels used in oil industry after stress corrosion cracking tests
- 2016The comparison of the microstructure and corrosion resistance of sand cast aluminum alloyscitations
- 2016Influence of the corrosive environment on the Portevin–Le Chatelier plastic instability phenomenon in Al–1Mg and Al–3Mg model alloys
- 2016Weight loss measurements of AZ31 as cast and after heat treatment with the use of neutral salt spray tests
- 2015Corrosion Behaviour of Magnesium Lithium Alloys in NaCl Solutioncitations
- 2014Influence of casting method and heat treatment for corrosion resistance of magnesium alloy AZ91D
Places of action
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article
In vitro and in vivo degradation behavior of Mg-0.45Zn-0.45Ca (ZX00) screws for orthopedic applications
Abstract
Magnesium (Mg) alloys have become a potential material for orthopedic implants due to their unnecessaryimplant removal, biocompatibility, and mechanical integrity until fracture healing. This study examined the invitro and in vivo degradation of an Mg fixation screw composed of Mg-0.45Zn-0.45Ca (ZX00, in wt.%). With ZX00human-sized implants, in vitro immersion tests up to 28 days under physiological conditions, along with electrochemicalmeasurements were performed for the first time. In addition, ZX00 screws were implanted in thediaphysis of sheep for 6, 12, and 24 weeks to assess the degradation and biocompatibility of the screws in vivo.Using scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDX), microcomputedtomography (μCT), X-ray photoelectron spectroscopy (XPS), and histology, the surface and crosssectionalmorphologies of the corrosion layers formed, as well as the bone-corrosion-layer-implant interfaces,were analyzed. Our findings from in vivo testing demonstrated that ZX00 alloy promotes bone healing and theformation of new bone in direct contact with the corrosion products. In addition, the same elemental compositionof corrosion products was observed for in vitro and in vivo experiments; however, their elemental distribution andthicknesses differ depending on the implant location. Our findings suggest that the corrosion resistance wasmicrostructure-dependent. The head zone was the least corrosion-resistant, indicating that the production procedurecould impact the corrosion performance of the implant. In spite of this, the formation of new bone and noadverse effects on the surrounding tissues demonstrated that the ZX00 is a suitable Mg-based alloy for temporarybone implants.