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Bai, Jianming
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article
High-temperature oxidation of advanced FeCrNi alloy in steam environments
Abstract
Alloys of iron-chromium-nickel are being explored as alternative cladding materials to improve safety margins under severe accident conditions. Here, our research focuses on non-destructively investigating the oxidation behavior of the FeCrNi alloy “Alloy 33” using synchrotron-based methods. The evolution and structure of oxide layer formed in steam environments were characterized using X-ray diffraction, hard X-ray photoelectron spectroscopy, X-ray fluorescence methods and scanning electron microscopy. In conclusion, our results demonstrate that a compact and continuous oxide scale was formed consisting of two layers, chromium oxide and spinel phase (FeCr<sub>2</sub>O<sub>4</sub>) oxides, wherein the concentration of the FeCr<sub>2</sub>O<sub>4</sub> phase decreased from the surface to the bulk-oxide interface.