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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Mozetic, Miran
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Topics
Publications (9/9 displayed)
- 2021Plasma mediated chlorhexidine immobilization onto polylactic acid surface via carbodiimide chemistry: Antibacterial and cytocompatibility assessmentcitations
- 2021Distribution of the Deposition Rates in an Industrial-Size PECVD Reactor Using HMDSO Precursorcitations
- 2019The effect of composition of a polymeric coating on the biofilm formation of bacteria and filamentous fungi ; Vliv složení polymerního povlaku na tvorbu biofilmu bakterií a vláknitých hubcitations
- 2014Oxidation of Inconel 625 superalloy upon treatment with oxygen or hydrogen plasma at high temperaturecitations
- 2013Preparation of active antibacterial LDPE surface through multistep physicochemical approach II: Graft type effect on antibacterial propertiescitations
- 2012Etching of polyethylene terephthalate thin films by neutral oxygen atoms in the late flowing afterglow of oxygen plasmacitations
- 2012A Catalytic Sensor for Measurement of Radical Density in CO2 Plasmascitations
- 2012Effect of Phase Arrangement on Solid State Mechanical and Thermal Properties of Polyamide 6/Polylactide Based Co-polyester Blendscitations
- 2012Recent Progress in Surface Modification of Polyvinyl Chloridecitations
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article
Oxidation of Inconel 625 superalloy upon treatment with oxygen or hydrogen plasma at high temperature
Abstract
International audience ; Initial stages of Inconel 625 superalloy (Ni60Cr30Mo10Ni4Nb1) oxidation upon short treatment with gaseous plasma at different temperatures up to about 1600 K were studied. Samples were treated for different periods up to a minute by oxygen or hydrogen plasma created with a microwave discharge in the standing-wave mode at a pressure of 40 Pa and a power 500 W. Simultaneous heating of the samples was realized by focusing concentrated solar radiation from a 5 kW solar furnace directly onto the samples. The morphological changes upon treatment were monitored using scanning electron microscopy, compositional depth profiling was performed using Auger electron spectroscopy, while structural changes were determined by X-ray diffraction. The treatment in oxygen plasma caused formation of metal oxide clusters of three dimensional crystallites initially rich in nickel oxide with the increasing chromium oxide content as the temperature was increasing. At about 1100 K iron and niobium oxides prevailed on the surface causing a drop of the material emissivity at 5 μm. Simultaneously the NiCr2O4 compound started growing at the interface between the oxide film and bulk alloy and the compound persisted up to temperatures close to the Inconel melting point. Intensive migration of minority alloying elements such as Fe and Ti was observed at 1600 K forming mixed surface oxides of sub-micrometer dimensions. The treatment in hydrogen plasma with small admixture of water vapor did not cause much modification unless the temperature was close to the melting point. At such conditions aluminum segregated on the surface and formed well-defined Al2O3 crystals.