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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Balat-Pichelin, Marianne J. H.
Laboratoire Procédés, Matériaux et Energie Solaire
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (26/26 displayed)
- 2021Metal fuels production through the solar carbothermal reduction of magnesia: Effect of the reducing agentcitations
- 2021Metallic fuels production through the solar carbothermal reduction of magnesia: effect of the reducing agent
- 2021Oxidation and high-temperature radiative properties of the Kanthal Super ER intermetallic alloycitations
- 2020Oxidation in air at 1400 K and optical properties of Inconel 625, FeCrAlloy and Kanthal Super ERcitations
- 2019Sintering and oxidation behavior of HfB2-SiC composites from 0 to 30 vol% SiC between 1450 and 1800 Kcitations
- 2019Sintering and oxidation behavior of HfB2-SiC composites from 0 to 30 vol% SiC between 1450 and 1800 Kcitations
- 2019High temperature oxidation behavior of fully dense ZrB2/SiC and HfB2/SiC ceramic composites with various compositions under atomic oxygen plasma
- 2019High temperature properties of AlN coatings deposited by chemical vapor deposition for solar central receiverscitations
- 2019Multilayer multifunctional advanced coatings for receivers of concentrated solar power plantscitations
- 2019High temperature chemical vapor deposition of aluminum nitride thin films and coatings: properties and applications
- 2018Comportement à l'oxydation des composites ultra-réfractaires (Hf/Zr)B2-SiC à très haute température et au cyclage
- 2018Thermal analysis on the AlSi12-SiC hybrid composites sintered using solar energy (poster)
- 2017Contribution à l'étude thermodynamique et comportement à l'oxydation de céramiques ultra-réfractaires à base de diborure d'hafnium et de carbure de silicium
- 2017Contribution to the thermodynamic study and oxidation behavior of HfB2-SiC Ultra-High Temperature Ceramics
- 2016Optical indices and transport scattering coefficient of pyrolytic boron nitride: a natural thermal barrier coating for solar shieldscitations
- 2016Optical indices and transport scattering coefficient of pyrolytic boron nitride: a natural thermal barrier coating for solar shieldscitations
- 2016Influence of surface roughness and temperature on the oxidation behavior of ZrC/SiC samplescitations
- 2015Oxidation at high temperature in air plasma for the TPS of IXV – Passive/active transition and temperature jump
- 2014Synthesis of iron-oxide nanowires using industrial-grade iron substratescitations
- 2014Oxidation of Inconel 625 superalloy upon treatment with oxygen or hydrogen plasma at high temperaturecitations
- 2014Aerothermal response of ceramic matrix composites to nitrogen plasma at temperatures above 2000 Kcitations
- 2014Oxidation behavior of spark plasma sintered ZrC–SiC composites obtained from the polymer-derived ceramics routecitations
- 2014XPS and AES studies of UHTC ZrB2-SiC-Si3N4 treated with solar energycitations
- 2014Emissivity, catalycity and microstructural characterization of ZrB2–SiCfiber based UHTC at high temperature in a non-equilibrium air plasma flowcitations
- 2012A Catalytic Sensor for Measurement of Radical Density in CO2 Plasmascitations
- 2012High temperature oxidation of SiC f /PyC/SiC composite in helium for the Gas-cooled Fast Reactor
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article
Oxidation of Inconel 625 superalloy upon treatment with oxygen or hydrogen plasma at high temperature
Abstract
International audience ; Initial stages of Inconel 625 superalloy (Ni60Cr30Mo10Ni4Nb1) oxidation upon short treatment with gaseous plasma at different temperatures up to about 1600 K were studied. Samples were treated for different periods up to a minute by oxygen or hydrogen plasma created with a microwave discharge in the standing-wave mode at a pressure of 40 Pa and a power 500 W. Simultaneous heating of the samples was realized by focusing concentrated solar radiation from a 5 kW solar furnace directly onto the samples. The morphological changes upon treatment were monitored using scanning electron microscopy, compositional depth profiling was performed using Auger electron spectroscopy, while structural changes were determined by X-ray diffraction. The treatment in oxygen plasma caused formation of metal oxide clusters of three dimensional crystallites initially rich in nickel oxide with the increasing chromium oxide content as the temperature was increasing. At about 1100 K iron and niobium oxides prevailed on the surface causing a drop of the material emissivity at 5 μm. Simultaneously the NiCr2O4 compound started growing at the interface between the oxide film and bulk alloy and the compound persisted up to temperatures close to the Inconel melting point. Intensive migration of minority alloying elements such as Fe and Ti was observed at 1600 K forming mixed surface oxides of sub-micrometer dimensions. The treatment in hydrogen plasma with small admixture of water vapor did not cause much modification unless the temperature was close to the melting point. At such conditions aluminum segregated on the surface and formed well-defined Al2O3 crystals.