| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Navarro-López, Alfonso
Delft University of Technology
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (7/7 displayed)
- 2021Phase-transformation and precipitation kinetics in vanadium micro-alloyed steels by in-situ, simultaneous neutron diffraction and SANScitations
- 2021Phase-transformation and precipitation kinetics in vanadium micro-alloyed steels by in-situ, simultaneous neutron diffraction and SANScitations
- 2020Furnace for in situ and simultaneous studies of nano-precipitates and phase transformations in steels by SANS and neutron diffractioncitations
- 2020Evolution of the precipitate composition during annealing of vanadium micro-alloyed steels by in-situ SANScitations
- 2019Interaction of precipitation with austenite-to-ferrite phase transformation in vanadium micro-alloyed steelscitations
- 2019Interaction of precipitation with austenite-to-ferrite phase transformation in vanadium micro-alloyed steels
- 2019Interaction of precipitation with austenite-to-ferrite phase transformation in vanadium micro-alloyed steelscitations
Places of action
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article
Evolution of the precipitate composition during annealing of vanadium micro-alloyed steels by in-situ SANS
Abstract
<p>In-situ Small-Angle Neutron Scattering (SANS) is used to determine the time evolution of the chemical composition of precipitates at 650 °C and 700 °C in three micro-alloyed steels with different vanadium (V) and carbon (C) concentrations. Precipitates with a distribution of substoichiometric carbon-to-metal ratios are measured in all steels. The precipitates are initially metastable with a high iron (Fe) content, which is gradually being substituted by vanadium during isothermal annealing. Eventually a plateau in the composition of the precipitate phase is reached. Faster changes in the precipitate chemical composition are observed at the higher temperature in all steels because of the faster vanadium diffusion at 700 °C. At both temperatures, the addition of more vanadium and more carbon to the steel has an accelerating effect on the evolution of the precipitate composition as a result of a higher driving force for precipitation. Addition of vanadium to the nominal composition of the steel leads to more vanadium rich precipitates, with less iron and a smaller carbon-to-metal ratio. Atom Probe Tomography (APT) shows the presence of precipitates with a distribution of carbon-to-metal ratios, ranging from 0.75 to 1, after 10 h of annealing at 650 °C or 700 °C in all steels. These experimental results are coupled to ThermoCalc equilibrium calculations and literature findings to support the Small-Angle Neutron Scattering results.</p>