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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Wahlmann, Benjamin
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2024Thermo‐mechanical Study on Auxetic Shape Memory Periodic Open Cellular Structures—Part II: Mechanical and Shape Memory Propertiescitations
- 2024Experimental Validation of Property Models and Databases for Computational Superalloy Design
- 2023Using Selective Electron Beam Melting to Enhance the High-Temperature Strength and Creep Resistance of NiAl–28Cr–6Mo In Situ Compositescitations
- 2023MiniMelt: An instrument for real-time tracking of electron beam additive manufacturing using synchrotron x-ray techniquescitations
- 2023Numerical Design of CoNi-Base Superalloys With Improved Casting Structurecitations
- 2023Phase-Field Study of the History-Effect of Remelted Microstructures on Nucleation During Additive Manufacturing of Ni-Based Superalloyscitations
- 2022Revealing dynamic processes in laser powder bed fusion with in situ X-ray diffraction at PETRA IIIcitations
- 2021Numerical Alloy Development for Additive Manufacturing towards Reduced Cracking Susceptibilitycitations
- 2019Growth and coarsening kinetics of gamma prime precipitates in CMSX-4 under simulated additive manufacturing conditionscitations
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article
Growth and coarsening kinetics of gamma prime precipitates in CMSX-4 under simulated additive manufacturing conditions
Abstract
Additive manufacturing of superalloys offers new opportunities for alloy design but also poses significant processing difficulties. While the γ′ phase is responsible for the excellent high-temperature resistance of these alloys, it also induces cracking by precipitation hardening during manufacturing. Using small-angle X-ray scattering, we characterized the dynamic precipitation, dissolution, coarsening, and morphological evolution of the γ′ phase in situ during simulated additive manufacturing conditions. For this purpose, a CMSX-4 cylinder was subjected to cyclic heat treatment with heating and quenching rates up to 300 K/s. A specialized setup employing aluminum lenses to focus the X-ray beam was utilized to extend the q-range to small scattering vectors up to 0.035 nm−1. It was shown that the γ′ phase precipitates extremely fast without any measurable undercooling but remains below the equilibrium fraction throughout the process. Coarsening is readily measurable over timespans of only several seconds. A fraction of the γ′ phase that was dissolved during heating reprecipitated by forming new particles instead of growing on already existing precipitates. The findings provide new insight into the dynamic behavior of the γ′ phase during additive manufacturing and may prove valuable in designing new superalloys and processing strategies for additive manufacturing.