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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Haberfehlner, Georg
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (13/13 displayed)
- 20232D and 3D STEM Imaging and Spectroscopy: Applications and Perspectives in View of Novel STEM Infrastructure
- 2023Large mechanical properties enhancement in ceramics through vacancy-mediated unit cell disturbancecitations
- 2023Spectral Tuning of Plasmonic Activity in 3D Nanostructures via High-Precision Nano-Printingcitations
- 2023The challenge with high permittivity acceptors in organic solar cells: a case study with Y-series derivativescitations
- 2022Quantifying Ordering Phenomena at the Atomic Scale in Rare Earth Oxide Ceramics via EELS Elemental Mapping
- 2022Challenges in the characterization of complex nanomaterials with analytical STEM
- 2021Spectroscopic STEM imaging in 2D and 3D
- 2020Study on Ca Segregation toward an Epitaxial Interface between Bismuth Ferrite and Strontium Titanatecitations
- 2020Ca segregation towards an in-plane compressive strain Bismuth Ferrite – Strontium Titanate interface
- 2019In situ real-time annealing of ultrathin vertical Fe nanowires grown by focused electron beam induced depositioncitations
- 2019Analyzing the Nanogranularity of Focused-Electron-Beam-Induced-Deposited Materials by Electron Tomographycitations
- 2016Formation of bimetallic clusters in superfluid helium nanodroplets analysed by atomic resolution electron tomography
- 2011Development of porosimetry techniques for the characterization of plasma-treated porous ultra low-K materialscitations
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article
In situ real-time annealing of ultrathin vertical Fe nanowires grown by focused electron beam induced deposition
Abstract
Focused Electron Beam Induced Deposition is a consolidated technique for the growth of three-dimensional (3D) nanostructures. However, this single-step nanofabrication method requires furtherefforts to optimize simultaneously dimensional and compositional properties, in particular for depositswith a high aspect ratio. More specifically, ferromagnetic 3D nanowires (NWs) with diameters in the sub-50 nm regime and high metallic contents up to 95 at. % attract great interest to improve thefinal per-formance of magnetic nanodevices such as magnetic tips for scanning probe microscopy. In this work, wereport on real-time monitoring during chemical purification and structural crystallization processes ofultra-narrow 3D Fe NWs (<50 nm in diameter achieved) by post-growthin situannealing in a trans-mission electron microscope. NW heating up to 700C in very high vacuum reveals the local increase ofthe metallic content along the entire NW length concomitant with the growth of large Fe single crystalsfrom initially amorphous compounds. A metallic purity of 95 at. % is observed in several regions,dramatically boosting the initial Fe content of 40 at. %. The real-timein situtracking of 3D nanostructuresduring thermal annealing is a key element to design and optimize novel purification processes for thefabrication of customized components to be integrated in spintronic, logic and sensing devices