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Znidar, Desiree
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article
Investigations on the continuous flow generation of 2,6-dichloro-N-fluoropyridinium tetrafluoroborate using F2 gas
Abstract
<jats:title>Abstract</jats:title><jats:p>An explorative study on the continuous flow generation of the N-F reagent 2,6-dichloro-1-fluoro-pyridinium tetrafluoroborate from 2-6-dichloropyridine and 10% F<jats:sub>2</jats:sub>/N<jats:sub>2</jats:sub> and its telescoped downstream electrophilic fluorination reaction with an enamine is reported. The 2-step procedure was performed in a modular lab-scale silicon carbide flow reactor, which safely allowed processing corrosive F<jats:sub>2</jats:sub> and precise temperature control. Both reaction sequences turned out to be very fast when carried out in flow at − 10 °C: the N-F generation step could be done within 7.9 s and only 6.6 s were necessary for the fluorination of the enamine.</jats:p><jats:p><jats:bold>Graphical abstract</jats:bold></jats:p>