• Gurau, Carmela
• Silva, Rui J. C.
• Marin, Florin
• Fernandes, Francisco Manuel Braz
• Gurau, Gheorghe

Abstract

<p>Recently, severe plastic deformation (SPD) is recognized as a very efficient processing technique for the fabrication of bulk nanostructured (ns)/ultrafine-grained materials. High-speed high-pressure torsion (HSHPT) process, an SPD method, is used as a novel approach to produce ultrafine grains in memory materials. The influence of HSHPT process variables on some Cu-based shape memory alloys (SMAs) is explored and discussed. This paper also envisages providing a comparative study of significant microstructural evolutions and features that are introduced by HSHPT processing. The plastic deformation mechanisms of the copper-based SMAs are investigated from macrostructural and microstructural points of view using optical and scanning electron microscopic techniques. In addition, significant grain size reduction brought about by the process is attested by X-ray diffraction and transmission electron microscopy. The transition temperatures have been determined by differential scanning calorimetry.</p>

Topics

• impedance spectroscopy
• polymer
• grain
• grain size
• x-ray diffraction
• transmission electron microscopy
• copper
• differential scanning calorimetry
• deformation mechanism