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García, Eduard
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article
The effect of volatiles on the measurement of the reaction heat by differential scanning calorimetry
Abstract
When gases evolve during a chemical reaction, a fraction of the reaction heat is lost with them. We have ana- lyzed, both theoretically and experimentally, the deviations that this effect can produce on the determination of the reac- tion heat by differential scanning calorimetry (DSC). It is shown that, even in the absence of gas overheating, deviations related to variations in the sample heat capacity can be sub- stantial in experiments involving very intense DSC peaks. However, experiments performed on thermal decomposition of metal organic salts and on evaporation of liquids have shown that deviations usually arise from gas overheating.