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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Shinde, Surendra
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Publications (15/15 displayed)
- 2017Structural, optical, and photoelectrochemical properties of nanosphere-like CdXZn1-XS synthesized by electrochemical routecitations
- 2017Electrochemical synthesis: Monoclinic Cu2Se nano-dendrites with high performance for supercapacitorscitations
- 2017Morphological modification of CdSe0.6Te0.4 nanostructures by electron irradiation and the effect on photoelectrochemical cellscitations
- 2016Morphological tuning of CuO nanostructures by simple preparative parameters in SILAR method and their consequent effect on supercapacitorscitations
- 2015Hierarchical 3D-flower-like CuO nanostructure on copper foil for supercapacitorscitations
- 2015Electrosynthesis of nanoflower like-ZnS thin films and its characterizationscitations
- 2015Temperature Dependence of Cationic and Anionic Precursor on Morphological Improvement of CuO Electrodes and Its Consequent Effect on Electrochemical Supercapacitive Propertiescitations
- 2014Structural, optical, and photo-electrochemical properties of marygold-like CdSe0.6Te0.4 synthesized by electrochemical routecitations
- 2014Morphological modulation of polypyrrole thin films through oxidizing agents and their concurrent effect on supercapacitor performancecitations
- 2014Architectured Morphologies of Chemically Prepared NiO/MWCNTs Nanohybrid Thin Films for High Performance Supercapacitorscitations
- 2013Porous CuO nanosheet clusters prepared by a surfactant assisted hydrothermal method for high performance supercapacitorscitations
- 2013Enhanced activity of chemically synthesized hybrid graphene oxide/Mn3O4 composite for high performance supercapacitorscitations
- 2013Temperature influence on morphological progress of Ni(OH)2 thin films and its subsequent effect on electrochemical supercapacitive propertiescitations
- 2013Electrochemical synthesis of photosensitive nano-nest like CdSe0.6Te0.4 thin filmscitations
- 2013One step hydrothermal synthesis of micro-belts like Beta-Ni(OH)2 thin films for supercapacitorscitations
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article
Electrosynthesis of nanoflower like-ZnS thin films and its characterizations
Abstract
The thin films of ZnS have been electrodeposited onto stainless steel and ITO coated glass substrate. The films were prepared in aqueous bath, using ZnSO<sub>4</sub> and Na<sub>2</sub>S<sub>2</sub>O<sub>3</sub> as a precursor. The PH of bath maintained throughout the experiment is ~14. The preparative conditions are optimized to get ZnS thin films. The prepared films were further characterized for the structural, morphological and optical properties by X-ray diffraction (XRD), FT-Raman, fourier transform infrared (FTIR) spectroscopy, field emission scanning electron microscope (FE-SEM), energy dispersive spectroscopy (EDAX), atomic force microscopy (AFM), optical absorption spectroscopy, surface wettability studies, respectively. The XRD study shows the formation of ZnS phase with polycrystalline in nature. The nanoflower like morphology is observed for ZnS thin film with thickness 63 nm. FT-IR spectrum of ZnS thin film, were used to investigate the presence of organic compounds, as impurities in the ZnS films. FT-Raman shows the crystal quality and vibration properties of ZnS thin films.The water contact angle measurement shows that the ZnS thin film is hydrophilic in nature. Moreover, the optical study revealed the band gap of 3.13 eV.