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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Campina, Jm
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (6/6 displayed)
- 2020A layered nanocomposite of laccase, chitosan, and Fe3O4 nanoparticles-reduced graphene oxide for the nanomolar electrochemical detection of bisphenol Acitations
- 2016Reduced graphene oxide-nickel nanoparticles/biopolymer composite films for the sub-millimolar detection of glucosecitations
- 2015Potentiostatic Electropolymerization of Triphenylamine: A Low-Cost Cathode for Solid-State Photovoltaicscitations
- 2013Ultrasound-assisted preparation of size-controlled chitosan nanoparticles: Characterization and fabrication of transparent biofilmscitations
- 2012Aggregation-induced conformational transitions in bovine beta-lactoglobulin adsorbed onto open chitosan structurescitations
- 2011Solid-state electropolymerization and doping of triphenylamine as a route for electroactive thin filmscitations
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article
A layered nanocomposite of laccase, chitosan, and Fe3O4 nanoparticles-reduced graphene oxide for the nanomolar electrochemical detection of bisphenol A
Abstract
A hybrid conjugate of reduced graphene oxide/ferrous-ferric oxide nanoparticles (rGO-Fe3O4 NPs) is characterized and assembled with chitosan and laccase to form a layered functional superstructure. After its characterization by field-effect scanning electron microscopy, energy-dispersive X-ray analysis, X-ray photoelectron spectroscopy, attenuated total reflectance Fourier transform infrared, cyclic voltammetry (CV), and electrochemical impedance spectroscopy (EIS), the nanocomposite has been deposited on glassy carbon for the enzyme-mediated electrochemical determination of the endocrine disruptor bisphenol A (BPA). Proof-of-concept assays conducted by using CV, EIS, and square wave voltammetry reveal that the enzymatic biosensor provides linear response in a wide range of BPA concentrations (6-228 ppb), very high sensitivities, and excellent durability (over 1-month storage). Using amperometric detection, remarkable sensitivities (2080 mu A mu M-1 cm(-2)) and detection limits (18 nM) are attained. Applications to real samples of bottled water proved feasible with recoveries in the range 107-124%.