| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Anderson, Michael W.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2018Facile isolation of a stable S 6 -symmetric methanol hexamer using the guest-free microporous metal-organic framework:Zinc 5-tert-butyl isophthalatecitations
- 2017Predicting crystal growth via a unified kinetic three-dimensional partition modelcitations
- 2014Structures of silica-based nanoporous materials revealed by microscopycitations
- 2014Silica-Based Nanoporous Materialscitations
- 2013Materials discovery and crystal growth of zeolite A type zeolitic-imidazolate frameworks revealed by atomic force microscopycitations
- 2013A review of fine structures of nanoporous materials as evidenced by microscopic methodscitations
- 2012Crystal growth mechanisms and morphological control of the prototypical metal-organic framework MOF-5 revealed by atomic force microscopycitations
- 2012Growth mechanism of microporous zincophosphate sodalite revealed by in situ atomic force microscopycitations
- 2011Revelation of the molecular assembly of the nanoporous metal organic framework ZIF-8citations
- 2010Assessing Molecular Transport Properties of Nanoporous Materials by Interference Microscopycitations
- 2008Combined MS and NMR: attractive route to future understanding of the first stages of nucleation of nanoporous materialscitations
- 2007Crystal growth in nanoporous framework materialscitations
Places of action
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article
Structures of silica-based nanoporous materials revealed by microscopy
Abstract
<p>Ordered nanoporous structures are among the most fascinating and industrially important materials currently in use. The archetypal zeolite material has now been joined by an eclectic array of new structures that exhibit porosity over a wide range of length scales and with order/disorder expressed in a multitude of ways. This raises the bar in terms of characterization and extends a real challenge to the scientific community to fully understand the properties and potential future applications of such materials. In this review we discuss the importance of modern microscopy tools combined with diffraction in this endeavour and show how the details of even the most complex quasi-crystalline nanoporous architectures can be elucidated. We show by using the appropriate spherical aberration (Cs) corrections in scanning transmission electron microscopy it is possible to decipher all the individual silicon and aluminum atoms in a zeolite structure. Automated routines for using large electron diffraction datasets for crystal structure determination of nanocrystals is described making the need for large single crystal synthesis less-and-less important. The power of complementary combinations of surface tools such as atomic force microscopy and high-resolution scanning electron microscopy is discussed to elucidate crystal growth mechanisms. For mesoporous materials synthesized from self-organized organic mesophases electron microscopy reveals the details of the complex hierarchy of porosity so crucial for the functional performance of the structure.</p>