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Webster, Michael
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article
Spectroscopic and Vanadium K-Edge EXAFS Studies on VO2Cl and the Crystal Structure of [{Cl2VO(O2PCl2)(POCl3)}2]
Abstract
Spectroscopic and vanadium K-edge EXAFS data on VO2Cl suggest a structure based upon a dimeric OClV(-O)2VClO core linked by longer V···Cl interactions into a polymer. The crystal structure of [{Cl2VO(O2PCl2)(POCl3)}2], obtained from VO2Cland POCl3, shows a centrosymmetric dimer with bridgingPO2Cl2 groups, and terminal POCl3 ligands O-coordinated to each vanadium atom. Cl14O8P4V2: Space group P, Z = 1, lattice dimensions at 120 K: a = 8.039(2), b = 8.1641(15), c = 10.308(3) Å, = 92.586(15), = 103.829(10), = 106.963(15)°; R1 = 0.065.