Materials Map

Discover the materials research landscape. Find experts, partners, networks.

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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Materials Map under construction

The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (1/1 displayed)

  • 2020A Novel Recyclable Ni/Cu/Fe Termetallic Nanocatalyst for the Synthesis of Propargylamines through the A<sup>3</sup>‐Coupling Reactions17citations

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Rafiee, Ezzat
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Daryanavard, Marzieh
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Ataei, Ali
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2020

Co-Authors (by relevance)

  • Rafiee, Ezzat
  • Daryanavard, Marzieh
  • Ataei, Ali
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article

A Novel Recyclable Ni/Cu/Fe Termetallic Nanocatalyst for the Synthesis of Propargylamines through the A<sup>3</sup>‐Coupling Reactions

  • Sheykhabadi, Parvan Ghaderi
  • Rafiee, Ezzat
  • Daryanavard, Marzieh
  • Ataei, Ali
Abstract

<jats:title>Abstract</jats:title><jats:p>A novel Ni/Cu/Fe nanocatalyst was prepared <jats:italic>via</jats:italic> a three‐step procedure for the A<jats:sup>3</jats:sup>‐coupling reaction of an aldehyde, an amine, and a terminal alkyne to synthesize the corresponding propargylamine. Oleic acid was used in the second step to avoid aggregation of CuFe<jats:sub>2</jats:sub>O<jats:sub>4</jats:sub> nanoparticles. The prepared <jats:bold>NiO/OA‐CuFe<jats:sub>2</jats:sub>O<jats:sub>4</jats:sub></jats:bold> (Ni/Cu/Fe) was characterized using X‐ray diffraction (XRD), scanning electron microscopy/wavelength dispersive X‐ray (SEM/WDX), particle size analyzer, fourier transform infrared (FT‐IR) and atomic absorption spectroscopy (AAS). A variety of propargylamines was synthesized using a very small amount of this efficient and inexpensive nanocatalyst in toluene as the solvent at 100 °C. Due to high magnetic properties of the prepared catalyst, its isolation and recycle were very easy, and it was used in five repetitive cycles.</jats:p>

Topics
  • nanoparticle
  • scanning electron microscopy
  • x-ray diffraction
  • amine
  • atomic absorpion spectrometry
  • alkyne
  • aldehyde