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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Guedes, Alexandra
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2024Highly Efficient and Magnetically Recyclable Non-Noble Metal Fly Ash-Based Catalysts for 4-Nitrophenol Reductioncitations
- 2024Graphitization: Microstructural and microtextural transformations of residual char from international coal combustion ashcitations
- 2024Graphitization: Microstructural and microtextural transformations of residual char from international coal combustion ashcitations
- 2023FoodSmarTag: An innovative dynamic labeling system based on pyranoflavylium-based colorimetric films for real-time monitoring of food freshnesscitations
- 2021Graphene@Metal Sulfide/Oxide Nanocomposites as Novel Photo-Fenton-like Catalysts for 4-Nitrophenol Degradationcitations
- 2020Hydrothermal Carbon/Carbon Nanotube Composites as Electrocatalysts for the Oxygen Reduction Reactioncitations
- 2018Electrochemical genoassays on gold-coated magnetic nanoparticles to quantify genetically modified organisms (GMOs) in food and feed as GMO percentagecitations
- 2018Photochromic polypropylene fibers based on UV-responsive silica@phosphomolybdate nanoparticles through melt spinning technologycitations
- 2018Petrographic and SEM/EDS characterization of bottom ash fractions obtained using magnetic separation equipment
- 2018Heteroatom-Doped Carbon Nanomaterials as Metal-Free Catalysts for the Reduction of 4-Nitrophenolcitations
- 2016Characterization of bottom ash of Pliocene lignite as ceramic composites raw material by petrographic, SEM/EDS and Raman microspectroscopical methodscitations
- 2014Tailored design of CoxMn1-xFe2O4 nanoferrites: a new route for dual control of size and magnetic propertiescitations
- 2014Gold nanoparticles decorated on Bingel-thiol functionalized multiwall carbon nanotubes as an efficient and robust catalystcitations
- 2012Multianalytical approaches to the characterisation of minerals associated with coals and the diagnosis of their potential risk by using combined instrumental microspectroscopic techniques and thermodynamic speciationcitations
- 2012Superparamagnetic MFe2O4 (M = Fe, Co, Mn) Nanoparticles: Tuning the Particle Size and Magnetic Properties through a Novel One-Step Coprecipitation Routecitations
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article
Heteroatom-Doped Carbon Nanomaterials as Metal-Free Catalysts for the Reduction of 4-Nitrophenol
Abstract
In this work it is described the preparation and characterization of multi-walled carbon nanotubes and graphene flakes doped with heteroatoms, namely N, P, B, and S, through simple ball milling procedures with adequate precursors, followed by thermal treatments. Ball milling the carbon nanomaterials with melamine resulted in the introduction of pyrrolic, pyridinic and quaternary N atoms on the graphitic structure. Using triphenylphosphine as the phosphorous precursor induced the formation of R-O-PO(OH)(2) functionalities. Materials prepared with boric acid showed the presence of boronic groups (C-BO2) and B atoms in B2O3. S-doped materials presented tiophene-S type atoms. The catalytic studies showed that all the doped carbon materials were active catalysts in the reduction of 4-nitrophenol (4-NP), and that the modifications introduced by the doping procedures, overall yielded catalysts with superior activity in regard to their pristine counterparts. Reusability experiments revealed no loss of catalytic activity up to three catalytic cycles for the doped carbon nanotubes, whereas the graphene flake materials showed some deterioration of catalytic performance.