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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Balat-Pichelin, Marianne J. H.
Laboratoire Procédés, Matériaux et Energie Solaire
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (26/26 displayed)
- 2021Metal fuels production through the solar carbothermal reduction of magnesia: Effect of the reducing agentcitations
- 2021Metallic fuels production through the solar carbothermal reduction of magnesia: effect of the reducing agent
- 2021Oxidation and high-temperature radiative properties of the Kanthal Super ER intermetallic alloycitations
- 2020Oxidation in air at 1400 K and optical properties of Inconel 625, FeCrAlloy and Kanthal Super ERcitations
- 2019Sintering and oxidation behavior of HfB2-SiC composites from 0 to 30 vol% SiC between 1450 and 1800 Kcitations
- 2019Sintering and oxidation behavior of HfB2-SiC composites from 0 to 30 vol% SiC between 1450 and 1800 Kcitations
- 2019High temperature oxidation behavior of fully dense ZrB2/SiC and HfB2/SiC ceramic composites with various compositions under atomic oxygen plasma
- 2019High temperature properties of AlN coatings deposited by chemical vapor deposition for solar central receiverscitations
- 2019Multilayer multifunctional advanced coatings for receivers of concentrated solar power plantscitations
- 2019High temperature chemical vapor deposition of aluminum nitride thin films and coatings: properties and applications
- 2018Comportement à l'oxydation des composites ultra-réfractaires (Hf/Zr)B2-SiC à très haute température et au cyclage
- 2018Thermal analysis on the AlSi12-SiC hybrid composites sintered using solar energy (poster)
- 2017Contribution à l'étude thermodynamique et comportement à l'oxydation de céramiques ultra-réfractaires à base de diborure d'hafnium et de carbure de silicium
- 2017Contribution to the thermodynamic study and oxidation behavior of HfB2-SiC Ultra-High Temperature Ceramics
- 2016Optical indices and transport scattering coefficient of pyrolytic boron nitride: a natural thermal barrier coating for solar shieldscitations
- 2016Optical indices and transport scattering coefficient of pyrolytic boron nitride: a natural thermal barrier coating for solar shieldscitations
- 2016Influence of surface roughness and temperature on the oxidation behavior of ZrC/SiC samplescitations
- 2015Oxidation at high temperature in air plasma for the TPS of IXV – Passive/active transition and temperature jump
- 2014Synthesis of iron-oxide nanowires using industrial-grade iron substratescitations
- 2014Oxidation of Inconel 625 superalloy upon treatment with oxygen or hydrogen plasma at high temperaturecitations
- 2014Aerothermal response of ceramic matrix composites to nitrogen plasma at temperatures above 2000 Kcitations
- 2014Oxidation behavior of spark plasma sintered ZrC–SiC composites obtained from the polymer-derived ceramics routecitations
- 2014XPS and AES studies of UHTC ZrB2-SiC-Si3N4 treated with solar energycitations
- 2014Emissivity, catalycity and microstructural characterization of ZrB2–SiCfiber based UHTC at high temperature in a non-equilibrium air plasma flowcitations
- 2012A Catalytic Sensor for Measurement of Radical Density in CO2 Plasmascitations
- 2012High temperature oxidation of SiC f /PyC/SiC composite in helium for the Gas-cooled Fast Reactor
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article
XPS and AES studies of UHTC ZrB2-SiC-Si3N4 treated with solar energy
Abstract
The microstructure of ultra-high-temperature ceramics based on the ZrB2–SiC composition and a sintering additive (Si3N4) was investigated using XPS and AES techniques. These ZrB2–SiC–Si3N4 materials were treated in air plasma at high temperature (T > 1750 K) in the MESOX facility developed at the PROMES-CNRS laboratory (Moyen d'Essai Solaire d'OXydation for the measurement of atomic oxygen recombination coefficients). The surfaces were characterized before and after the air plasma treatment. Surface modifications were observed and induced by the oxidation process. The elementary composition was determined using AES and XPS. Core level spectroscopy (XPS) was used to determine the atomic composition and the nature of the chemical bonds from the Zr 3d3/2,5/2, Si 2p1/2,3/2, O 1s and C 1s photoelectron peaks. The microstructural analyses revealed the presence of oxide layers: Silica and zirconia compounds were detected at temperatures near 1800 K, and a zirconia compound was mainly detected above 2200 K.