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Fernandes, Susete
Universidade Nova de Lisboa
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (8/8 displayed)
- 2017Hybrid polysaccharide-based systems for biomedical applicationscitations
- 2015Functional materials from liquid crystalline cellulose derivatives: Synthetic routes, characterization and applicationscitations
- 2014Cellulose‐Based Liquid Crystalline Composite Systemscitations
- 2014Nanocrystalline cellulose applied simultaneously as the gate dielectric and the substrate in flexible field effect transistorscitations
- 2005Synthesis of acrylamide end-functionalised poly(1-hexene) using an α-diimine nickel catalystcitations
- 2005Titanium and zirconium ketimide complexescitations
- 2005Photodegradation of ethylene/propylene/polar monomers co- and terpolymers. I - Prepared by group 4 catalyst systems
- 2002Polymerisation of ethylene catalysed by mono-imine-2,6-diacetylpyridine iron/methylaluminoxane (MAO) catalyst systemcitations
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article
Synthesis of acrylamide end-functionalised poly(1-hexene) using an α-diimine nickel catalyst
Abstract
<p>The nickel precursor [bis(N,N′-dimesitylimino acenaphthene]dibromonickel and methylaluminoxane were used to catalyse the functionalisation of 1-hexene with acrylamide by passivation of acrylamide with tri-isobutylaluminium. The polymer obtained was characterised by GPC/SEC and NMR. The NMR experiments performed, COSY, DEPT, long-range selective INEPT, HSQC and TOCSY 1D, showed that a 2,1 insertion of a single molecule of acrylamide per macromolecule had occurred at the end of the polyhexene chain.</p>