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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Hao, X.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (6/6 displayed)
- 2016Giant spin-torque diode sensitivity at low input power in theabsence of bias magnetic fieldcitations
- 2010Monitoring microstructure changes in rod online by using induction spectroscopycitations
- 2004Molecular composite materials formed from block copolymers containing a side-chain liquid crystalline segment and an amorphous styrene/maleic anhydride segmentcitations
- 2004Reversible addition fragmentation chain transfer polymerization of sterically hindered monomers: Toward well-defined rod/coil architecturescitations
- 2004Dendrimers as scaffolds for multifunctional reversible addition-fragmentation chain transfer agents: Syntheses and polymerizationcitations
- 2003A New Chemo-Enzymatic Route to Side-Chain Liquid-Crystalline Polymers: The Synthesis and Polymerization of 6-(4-Methoxybiphenyl-4′-oxy)hexyl Vinyl Hexanedioatecitations
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article
A New Chemo-Enzymatic Route to Side-Chain Liquid-Crystalline Polymers: The Synthesis and Polymerization of 6-(4-Methoxybiphenyl-4′-oxy)hexyl Vinyl Hexanedioate
Abstract
A novel synthetic method combining chemo and enzymatic synthesis strategies was employed to prepare a vinyl acetate type monomer, 6-(4-methoxybiphenyl-4′-oxy)hexyl vinyl hexanedioate (VA-LC). Homo- and copolymers of VA-LC with maleic anhydride (MAn) were prepared by conventional free radical polymerization using 2,2′-azobisisobutyronitrile (AIBN) and 1,1′-azobis (cyclohexane carbonitrile) (AHCN) as an initiator at 95 and 60 °C, respectively. The thermal properties of the generated polymeric material were investigated by differential scanning calorimetry (DSC), and the optical texture was inspected by polarizing optical microscopy (POM). While the monomer VA-LC does not exhibit liquid-crystalline properties, poly(VA-LC), and the alternating copolymer of VA-LC with maleic anhydride both displayed such properties.