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Bell, Andrew
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Publications (7/7 displayed)
- 2022Exploring domain continuity across BaTiO 3 grain boundaries: theory meets experimentcitations
- 2022Exploring domain continuity across BaTiO3 grain boundaries: Theory meets experimentcitations
- 2020Large scale sequencing of SARS-CoV-2 genomes from one region allows detailed epidemiology and enables local outbreak managementcitations
- 2017Polymers of norbornenyl‐4‐phenol: Dissolution rate characteristics, positive tone photo‐patterning, and polymer propertiescitations
- 2015A Microstructural Study on the Observed Differences in Charpy Impact Behavior Between Hot Isostatically Pressed and Forged 304L and 316L Austenitic Stainless Steelcitations
- 2011Brittle creep in basalt: implications for time-dependent volcano deformation
- 20084.4,5,5-tetraphenyl-1,3,2-dioxaborolanecitations
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article
4.4,5,5-tetraphenyl-1,3,2-dioxaborolane
Abstract
4,4,5,5-Tetraphenyl-1,3,2-dioxaborolane (HBBzpin, 3) has been prepared in high yield by the addition of H3B-SMe2 to benzopinacol. HBBzpin is a relatively stable solid that reacts with a variety of alkenes under catalytic conditions to give air- and chromatography-stable organoboronate esters. Reactions of vinylarenes in the presence of catalytic amounts of [Cp * IrCl2](2) gave the corresponding terminal products selectively. Addition of HBBzpin to RhCl(PPh3)(3) gave Rh(H)Cl(BzBpin)(PPh3)(2) (11) as the only new rhodium-containing product. The complex 11 has been characterized by a number of physical and analytical methods, including a single-crystal X-ray diffraction study. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008).