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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Hansen, Thomas
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (13/13 displayed)
- 2024Newly developed aerodynamic levitation device for neutron scattering experiments
- 2024Impact of Mn/Ni and Li/(Mn+Ni) ratios on phase equilibrium and electrochemical performance of the high voltage spinel LiNi0.5Mn1.5O4citations
- 2023Magnetic and structural properties of the iron silicide superconductor LaFeSiH
- 2022An Easy-to-Use Custom-Built Cell for Neutron Powder Diffraction Studies of Rechargeable Batteriescitations
- 2022An Easy‐to‐Use Custom‐Built Cell for Neutron Powder Diffraction Studies of Rechargeable Batteriescitations
- 2021Investigation into the magnetic properties of CoFeNiCryCux alloyscitations
- 2021Investigation into the magnetic properties of CoFeNiCryCux alloyscitations
- 2020High-pressure, high temperature synthesis of a mesoporous α-quartz/bismuth nanowire compositecitations
- 2020Structural Characteristics of Fresh, Thermally Aged, Poisoned and Regenerated Pt-Pd Catalysts Studied by Analytical Transmission Electron Microscopy
- 2019High-pressure, high temperature insertion of bismuth in the siliceous zeolite silicalite-1citations
- 2017Absence of magnetic long range order in Y2CrSbO7: bond-disorder induced magnetic frustration in a ferromagnetic pyrochlorecitations
- 2015Expression, receptor binding, and biophysical characterization of guinea pig insulin desB30citations
- 2013Reduction of Sr2MnO4 investigated by high temperature in situ neutron powder diffraction under hydrogen flow.citations
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article
An Easy‐to‐Use Custom‐Built Cell for Neutron Powder Diffraction Studies of Rechargeable Batteries
Abstract
In operando powder diffraction remains one of the most powerful tools for non‐destructive investigation of battery electrode materials. While in operando X‐ray, especially synchrotron radiation, powder diffraction is by now a routine experimental technique, in operando neutron powder diffraction is still less established. We present a new electrochemical cell for in operando neutron powder diffraction, which is, first and foremost, easy to use, but can also cycle electrode materials under electrochemical conditions close to those achieved using standard laboratory cells. The cell has been designed in multiple sizes, and high‐quality electrochemical and neutron powder diffraction data is presented for sample sizes as low as 48 mg total active material. The cell handles lithium‐ion and sodium‐ion materials equally well, with no difference in how the cell is prepared and assembled. The cell is intended to be used as sample environment at powder diffractometers at the neutron facilities MLZ, ORNL and ACNS. An in operando neutron powder diffraction cell was developed for research on battery electrodes using a simple design. The cell is optimized for a strong diffraction signal for small sample sizes. It is suitable for multiple battery chemistries and is aimed at research on novel materials. ; In operando powder diffraction remains one of the most powerful tools for non-destructive investigation of battery electrode materials. While in operando X-ray, especially synchrotron radiation, powder diffraction is by now a routine experimental technique, in operando neutron powder diffraction is still less established. We present a new electrochemical cell for in operando neutron powder diffraction, which is, first and foremost, easy to use, but can also cycle electrode materials under electrochemical conditions close to those achieved using standard laboratory cells. The cell has been designed in multiple sizes, and high-quality electrochemical and neutron powder diffraction data is presented for sample sizes as low as 48 ...