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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Mørch, Mathias I.
Aarhus University
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (10/10 displayed)
- 2024Aligned Permanent Magnet Made in Seconds–An In Situ Diffraction Studycitations
- 2024Aligned Permanent Magnet Made in Seconds:An In Situ Diffraction Studycitations
- 2023Sintering in seconds, elucidated by millisecond in situ diffractioncitations
- 2022Exploiting different morphologies of non-ferromagnetic interacting precursor’s for preparation of hexaferrite magnetscitations
- 2022Combined characterization approaches to investigate magnetostructural effects in exchange-spring ferrite nanocomposite magnetscitations
- 2021‘Need for Speed’: Sub-second in situ diffraction to unravel rapid sintering & texture evolution in ferrite magnets
- 2021‘Need for Speed’: Sub-second in situ diffraction to unravel rapid sintering & texture evolution in ferrite magnets
- 2019Novel fast heating furnaces for in situ powder neutron diffraction
- 2019Structure and magnetic properties of W-type hexaferritescitations
- 2019Novel in situ powder neutron diffraction setups – The creation of a modern magnetic compound
Places of action
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article
Aligned Permanent Magnet Made in Seconds–An In Situ Diffraction Study
Abstract
The synthesis of a strontium hexaferrite magnet is studied using in situ synchrotron powder X-ray diffraction (PXRD) with a 16-ms time resolution. The precursor material is cold compacted shape-controlled goethite and strontium carbonate. The time evolution of the phases is modeled with sequential Rietveld refinements revealing that strontium hexaferrite forms within seconds at ≈1173 K. Texture analysis is performed on selected PXRD frames throughout the experiment, and the preferred orientation introduced by cold-pressing goethite prevails through the iron oxide phase transitions (goethite → hematite → strontium hexaferrite). Electron backscatter diffraction (EBSD) data on the final pellet confirms the preferred orientation observed with PXRD. The resulting magnet has respectable magnetic properties, considering the simplicity of the preparation method, with an energy product (BHmax) of 18.6(8) kJ m−3.