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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Dahl, Vedrana Andersen
Technical University of Denmark
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (10/10 displayed)
- 2023Dataset for scanning electron microscopy based local fiber volume fraction analysis of non-crimp fabric glass fiber reinforced compositescitations
- 2023Elucidating the Bulk Morphology of Cellulose-Based Conducting Aerogels with X-Ray Microtomography
- 2023Elucidating the Bulk Morphology of Cellulose-Based Conducting Aerogels with X-Ray Microtomography
- 2022SparseMeshCNN with Self-Attention for Segmentation of Large Meshescitations
- 2021Quantifying effects of manufacturing methods on fiber orientation in unidirectional composites using structure tensor analysiscitations
- 2020Characterization of the fiber orientations in non-crimp glass fiber reinforced composites using structure tensorcitations
- 2019Process characterization for molding of paper bottles using computed tomography and structure tensor analysis
- 2019Fiber segmentation from 3D X-ray computed tomography of composites with continuous textured glass fibre yarns
- 2019Structural Characterization of Membrane-Electrode-Assemblies in High Temperature Polymer Electrolyte Membrane Fuel Cellscitations
- 2014Surface Detection using Round Cutcitations
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article
Elucidating the Bulk Morphology of Cellulose-Based Conducting Aerogels with X-Ray Microtomography
Abstract
Conducting cellulose composites are promising sustainable functional materials that have found application in energy devices, sensing and water purification. Herein, conducting aerogels are fabricated based on nanofibrillated cellulose and poly(3,4-ethylenedioxythiophene) polystyrene sulfonate, using the ice templating technique, and their bulk morphology is characterized with X-ray microtomography. The freezing method (−20 °C in a freezer vs liquid nitrogen) does not impact the mean porosity of the aerogels but the liquid-N<sub>2</sub> aerogels have smaller pores. The integration of carbon fibers as addressing electrodes prior to freezing results in increased mean porosity and pore size in the liquid-N<sub>2</sub> aerogels signifying that the carbon fibers alter the morphology of the aerogels when the freezing is fast. Spatially resolved porosity and pore size distributions also reveal that the liquid-N2 aerogels are more inhomogeneous. Independent of the freezing method, the aerogels have similar electrochemical properties. For aerogels without carbon fibers, freezer-aerogels have higher compression modulus and are less stable under cycling compression fatigue test. This can be explained by higher porosity with larger pores in the center of liquid-N<sub>2</sub> aerogels and thinner pore walls. This work demonstrates that micro-CT is a powerful tool for characterizing the morphology of aerogels in a non-destructive and spatially resolved manner.