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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Ressel, Gerald
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Topics
Publications (11/11 displayed)
- 2024Effect of intercritical annealing on the microstructure and mechanical properties of a PH 13-8 Mo maraging steelcitations
- 2024Multiscale in-situ observations of the micro- and nanostructure of a PH 13-8 Mo maraging steel during austenitizationcitations
- 2024Peculiarity of hydrogen absorption in duplex steels: Phase-selective lattice swelling and stress evolutioncitations
- 2023Design of Laves phase-reinforced compositionally complex alloycitations
- 2023In Situ Observations of the Microstructural Evolution during Heat Treatment of a PH 13-8 Mo Maraging Steelcitations
- 2022Influence of delta ferrite on the impact toughness of a PH 13-8 Mo maraging steelcitations
- 2022Influence of Tempering on Macro- and Micro-Residual Stresses and Yield Stress of Ferritic-Pearlitic Drawn, Coiled, and Straightened Wirescitations
- 2021Copper and its effects on microstructure and correlated tensile properties of super duplex stainless steelscitations
- 2019Formation of "carbide-free zones" resulting from the interplay of C redistribution and carbide precipitation during bainitic transformationcitations
- 2019In situ analysis of the effect of high heating rates and initial microstructure on the formation and homogeneity of austenitecitations
- 2018Different Cooling Rates and Their Effect on Morphology and Transformation Kinetics of Martensitecitations
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article
In Situ Observations of the Microstructural Evolution during Heat Treatment of a PH 13-8 Mo Maraging Steel
Abstract
<p>The standard heat treatment of PH 13-8 Mo maraging steels consists of solution annealing and subsequent aging. Herein, it is investigated how an additional intercritical annealing step prior to aging affects the microstructure, and, consequently, the mechanical properties of a PH 13-8 Mo maraging steel. In situ techniques by means of high-temperature electron backscatter diffraction and high-temperature X-ray diffraction are applied to study the microstructural changes during intercritical annealing and subsequent aging. In addition, high-resolution investigation methods, such as transmission electron microscopy and atom probe tomography supplemented by transmission Kikuchi diffraction, are used for an in-depth characterization of the microstructure. The results reveal that a diffusion-controlled martensite to austenite transformation accompanied by partitioning of the substitutional atoms Cr, Ni, and Mo takes place during intercritical annealing. As a result of partitioning during intercritical annealing, an inhomogeneous distribution of Ni remains in the microstructure after the martensitic transformation. Consequently, the formation of reverted austenite is facilitated during subsequent aging due to existing Ni-enriched zones in martensite. Since the fracture toughness is significantly enhanced compared to the standard heat treatment, it is suggested that this improvement is related to the increased phase fraction of reverted austenite.</p>