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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Boudet, Nathalie
Processes and Engineering in Mechanics and Materials
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (24/24 displayed)
- 2023Influence of the Ge content on the lithiation process of crystalline Si 1− x Ge x nanoparticle-based anodes for Li-ion batteriescitations
- 2022Relationship between atomic structure and excellent glass forming ability in Pd 42.5 Ni 7.5 Cu 30 P 20 metallic glasscitations
- 2022Coupling between elastic strains and phase transition in dense pure zirconia polycrystalscitations
- 2022Relationship between atomic structure and excellent glass forming ability in Pd42.5Ni7.5Cu30P20 metallic glasscitations
- 2021Detailed structural analysis of amorphous Pd40Cu40P20: Comparison with the metallic glass Pd40Ni40P20 from the viewpoint of glass forming abilitycitations
- 2021Detailed structural analysis of amorphous Pd 40 Cu 40 P 20 :Comparison with the metallic glass Pd 40 Ni 40 P 20 from the viewpoint of glass forming abilitycitations
- 2020Prelithiation of silicon/graphite composite anodes: Benefits and mechanisms for long-lasting Li-Ion batteriescitations
- 2019Advanced Non-Destructive in Situ Characterization of Metals with the French Collaborating Research Group D2AM/BM02 Beamline at the European Synchrotron Radiation Facilitycitations
- 2019Advanced Non-Destructive in Situ Characterization of Metals with the French Collaborating Research Group D2AM/BM02 Beamline at the European Synchrotron Radiation Facilitycitations
- 2019Heterogeneous Nanostructural Aging of Fuel Cell Ionomer Revealed by Operando SAXScitations
- 2019Partial structure investigation of the traditional bulk metallic glass Pd40Ni40P20citations
- 2019Partial structure investigation of the traditional bulk metallic glass Pd40Ni40 P20citations
- 2018In situ Synchrotron X-Ray diffraction study of high-temperature stress relaxation in chromia scales containing the reactive element yttriumcitations
- 2017Strains in thermally growing Cr2O3 films measured in situ using synchrotron X-rayscitations
- 2016Tuning the conductivity type in a room temperature magnetic oxide: Ni-doped Ga0.6Fe1.4O3 thin filmscitations
- 2016Reaction of Ni film with In0.53Ga0.47As: Phase formation and texturecitations
- 2016Determination of the cationic distribution in oxidic thin films by resonant X-ray diffraction: the magnetoelectric compound Ga2-xFexO3. Supporting information
- 2016Self-organized arrays of dislocations in thin smectic liquid crystal filmscitations
- 2016Self-organized arrays of dislocations in thin smectic liquid crystal filmscitations
- 2014Probing Self-Assembly of Cylindrical Morphology Block Copolymer Using in Situ and ex Situ Grazing Incidence Small-Angle X-ray Scattering: The Attractive Case of Graphoepitaxycitations
- 2012Key experimental information on intermediate-range atomic structures in amorphous Ge2Sb2Te5 phase change materialcitations
- 2012Anomalous x-ray diffraction measurements of long-range order in (001)-textured L1(0) FePtCu thin filmscitations
- 2011Microstructural mapping of C60 phase transformation into disordered graphite at high pressure, using X-ray diffraction microtomographycitations
- 2007Development of structural order during supercooling of a fragile oxide meltcitations
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article
Strains in thermally growing Cr2O3 films measured in situ using synchrotron X-rays
Abstract
This work takes place in the general context of a better understanding of materials degradation mechanisms in extreme environments. In particular, the aim of the present study was to correlate microstructural elements to growth stress magnitude evolution and stress release mechanisms for thermally grown chromia thin films on NiCr alloys. Strains in thermally grown oxides have been measured in-situ, as the oxides develop and evolve. Data have been acquired from oxides grown for different high temperatures evolutions on NiCr model alloys that form Cr2O3. Using synchrotron X-Ray at the ESRF (Beamline BM02) coupled with an induction furnace, Debye-Scherrer diffraction patterns from the oxidizing specimen were recorded in air at temperature between 700-1000°C and during cooling. The distortion of the diffraction rings was analyzed to yield the in-plane strain. Thermal stresses imposed on Cr2O3/NiCr by abruptly reducing the sample temperature for a period of time, exploiting the thermal expansion difference between oxide and substrate, showed noticeable subsequent stress relaxation by creep. Such a mechanism was monitored using time-dependent in situ measurements of strain relaxation in the oxide. The main results obtained from these experiments are the kinetic of the growth stress from the isothermal measurements (isothermal plateau), and the study of the stress release mechanism after the low-temperature jumps. In complement, the oxide microstructure development during the course of oxidation is also investigated from both the peaks intensity and width evolution. In all cases, the steady stage growth strain was relatively low and compressive. Different degrees of relaxation were also found on cooling depending on scale microstructure through the variation of the initial oxidation conditions. Results are compared with other reports of residual stresses evolution in Cr2O3 scales. © 2017 Trans Tech Publications, Switzerland.