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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kočí, Jan | Prague |
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Müller, Thomas
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Topics
Publications (9/9 displayed)
- 2023Effect of deposition temperature and hydrogen as a process gas on mechanical properties and specific electrical resistivity of thick a-C:H obtained by means of PACVD
- 2022A Fluoroponytailed NHC–Silver Complex Formed from Vinyl-imidazolium/AgNO3 under Aqueous– Ammoniacal Conditionscitations
- 2021Growth, structure and stability of sputter-deposited MoS2 thin filmscitations
- 2020Neural control variatescitations
- 2017High temperature particle jet erosion of nickel- and cobalt-based alloys
- 2017Order and disorder in the charge and spin structures of $YFe_{2}O_{4}-delta$ and $Ni_{0.42}Mn_{0.58}TiO_{3}$
- 2017Carbon Nanoparticle‐Reinforced Metal Matrix Composites: Microstructural Tailoring and Predictive Modeling
- 2010The influence of the additive BaGeO3 on BaSnO3 ceramicscitations
- 2008Heavy-fermion behavior and spin-glass freezing in Si-stabilized amorphous alloys based on UPt3citations
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article
A Fluoroponytailed NHC–Silver Complex Formed from Vinyl-imidazolium/AgNO3 under Aqueous– Ammoniacal Conditions
Abstract
Publisher Copyright: © 2022 by the authors. Licensee MDPI, Basel, Switzerland. ; 3-(1H,1H,2H,2H-Perfluorooctyl)-1-vinylimidazolium chloride [2126844–17–3], a strong fluorosurfactant with remarkably high solubility in water, was expediently converted into the respective doubly NHC-complexed silver salt with nitrate as counter ion in quantitative yield. Due to its vinyl substituents, [bis(3-(1H,1H,2H,2H-perfluorooctyl)-1-vinylimidazol-2-ylidene)silver(I)] nitrate, Ag(FNHC)2NO3, represents a polymerizable N-heterocyclic carbene transfer reagent, thus potentially offering simple and robust access to coordination polymers with crosslinking metal bridges. The compound was characterized by infrared and NMR spectroscopy, mass spectrometry as well as elemental analysis, and supplemented by X-ray single-crystal structure determination. It crystallizes in the monoclinic crystal system in the space group P21/c. With 173.3◦, the geometry of the Ag-carbene bridge deviates slightly from linearity. The disordered perfluoroalkyl side chains exhibit a helical conformation. ; Peer reviewed