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Wagner, Michael
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Publications (7/7 displayed)
- 2023Matching the photocurrent of 2‐terminal mechanically‐stacked perovskite/organic tandem solar modules by varying the cell widthcitations
- 2023Electrochemical Conversion of Cu Nanowire Arrays into Metal-Organic Frameworks HKUST-1citations
- 2018Biodegradation of synthetic polymers in soilscitations
- 2018Sustainable conversion of lignocellulose to high-purity, highly crystalline flake potato graphite.citations
- 2018Establishing a Rodent Model of Ventricular Fibrillation Cardiac Arrest With Graded Histologic and Neurologic Damage With Different Cardiac Arrest Durationscitations
- 2016Cross-Cultural Depression Recognition from Vocal Biomarkerscitations
- 2014NanoSIMS combined with fluorescence microscopy as a tool for subcellular imaging of isotopically labeled platinum-based anticancer drugscitations
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article
Electrochemical Conversion of Cu Nanowire Arrays into Metal-Organic Frameworks HKUST-1
Abstract
<jats:p>We explore the conversion of free-standing Cu nanowire arrays produced by electrodeposition in polymer etched ion-track membranes into metal-organic frameworks KHUST-1 by electrochemical oxidation. HKUST-1 particles are built up when the as-formed Cu<jats:sup>2+</jats:sup> ions bind to the benzene tricarboxylic acid ligands (BTC<jats:sup>3−</jats:sup>) in the electrolyte solution. The morphology and crystallinity of the samples at different transformation stages are investigated by scanning and transmission electron microscopy. X-ray diffraction data taken at different conversion times confirm the formation of HKUST-1 particles. The conversion process resulted in octahedral structures of several <jats:italic>μ</jats:italic>m in size. Comparison of the Raman spectra with the band positions derived from density functional theory (DFT) calculations, suggests that vibrations involving Cu atoms appear only below 490 cm<jats:sup>−1</jats:sup> wavenumbers and involve the entire HKUST-1 lattice rather than vibrations of single bonds.</jats:p><jats:p><jats:inline-formula><jats:inline-graphic xmlns:xlink="http://www.w3.org/1999/xlink" xlink:href="jesacbba4-ga.jpg" xlink:type="simple" /></jats:inline-formula></jats:p>